(E)-4-methyl-1-phenyl-2-(phenylsulfonyl)pent-1-en-3-yl triisopropylsilyl ether

Base Information

Chemical Name:(E)-4-methyl-1-phenyl-2-(phenylsulfonyl)pent-1-en-3-yl triisopropylsilyl ether
CAS No.:145098-88-0
Molecular Formula:C₂₇H₄₀O₃SSi
Molecular Weight:472.764
Hs Code.:

Synonyms:(E)-4-methyl-1-phenyl-2-(phenylsulfonyl)pent-1-en-3-yl triisopropylsilyl ether

Suppliers and Price of (E)-4-methyl-1-phenyl-2-(phenylsulfonyl)pent-1-en-3-yl triisopropylsilyl ether

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-4-methyl-1-phenyl-2-(phenylsulfonyl)pent-1-en-3-yl triisopropylsilyl ether

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Technology Process of (E)-4-methyl-1-phenyl-2-(phenylsulfonyl)pent-1-en-3-yl triisopropylsilyl ether

There total 3 articles about (E)-4-methyl-1-phenyl-2-(phenylsulfonyl)pent-1-en-3-yl triisopropylsilyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 80522-42-5
triisopropylsilyl trifluoromethanesulfonate

: 145098-85-7
(E)-4-methyl-1-phenyl-2-(phenylsulfonyl)pent-1-en-3-ol

: 145098-88-0
(E)-4-methyl-1-phenyl-2-(phenylsulfonyl)pent-1-en-3-yl triisopropylsilyl ether

Guidance literature:: With 2,6-dimethylpyridine; In dichloromethane; 1.) -78 deg C, 2 h, 2.) room temperature, overnight;

Reference yield:

: 16212-06-9
phenyl styryl sulfone

: 145098-88-0
(E)-4-methyl-1-phenyl-2-(phenylsulfonyl)pent-1-en-3-yl triisopropylsilyl ether

Guidance literature:: Multi-step reaction with 2 steps

1: 42 percent / MeLi, MgBr₂ / diethyl ether; tetrahydrofuran; toluene / 1.) -95 - -65 deg C, 30 min, 2.) -80 deg C, 30 min, 3.) -45 deg C to room temperature

2: 92 percent / 2,6-lutidine / CH₂Cl₂ / 1.) -78 deg C, 2 h, 2.) room temperature, overnight

With 2,6-dimethylpyridine; methyllithium; magnesium bromide; In tetrahydrofuran; diethyl ether; dichloromethane; toluene;