(E)-(5-(2-(4-cyano-5-(dicyanomethylene)-2,2-dimethyl-2,5-dihydrofuran-3-yl)vinyl)-2-phenylbenzofuran-3-yl)mercury(II) chloride

Base Information

Chemical Name:(E)-(5-(2-(4-cyano-5-(dicyanomethylene)-2,2-dimethyl-2,5-dihydrofuran-3-yl)vinyl)-2-phenylbenzofuran-3-yl)mercury(II) chloride
CAS No.:1423718-98-2
Molecular Formula:C₂₆H₁₆ClHgN₃O₂
Molecular Weight:638.475
Hs Code.:

Synonyms:(E)-(5-(2-(4-cyano-5-(dicyanomethylene)-2,2-dimethyl-2,5-dihydrofuran-3-yl)vinyl)-2-phenylbenzofuran-3-yl)mercury(II) chloride

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Chemical Property of (E)-(5-(2-(4-cyano-5-(dicyanomethylene)-2,2-dimethyl-2,5-dihydrofuran-3-yl)vinyl)-2-phenylbenzofuran-3-yl)mercury(II) chloride

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Technology Process of (E)-(5-(2-(4-cyano-5-(dicyanomethylene)-2,2-dimethyl-2,5-dihydrofuran-3-yl)vinyl)-2-phenylbenzofuran-3-yl)mercury(II) chloride

There total 2 articles about (E)-(5-(2-(4-cyano-5-(dicyanomethylene)-2,2-dimethyl-2,5-dihydrofuran-3-yl)vinyl)-2-phenylbenzofuran-3-yl)mercury(II) chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1423718-97-1
(E)-2-(3-cyano-4-(4-hydroxy-3-(phenylethynyl)styryl)-5,5-dimethylfuran-2(5H)-ylidene)malononitrile

: 1423718-98-2
(E)-(5-(2-(4-cyano-5-(dicyanomethylene)-2,2-dimethyl-2,5-dihydrofuran-3-yl)vinyl)-2-phenylbenzofuran-3-yl)mercury(II) chloride

Guidance literature:: With mercury dichloride; In water; dimethyl sulfoxide; at 25 ℃; for 3h;
DOI:10.1021/ol4000873

Reference yield:

: 536-74-3
phenylacetylene

: 1423718-98-2
(E)-(5-(2-(4-cyano-5-(dicyanomethylene)-2,2-dimethyl-2,5-dihydrofuran-3-yl)vinyl)-2-phenylbenzofuran-3-yl)mercury(II) chloride

Guidance literature:: Multi-step reaction with 3 steps

1: copper(l) iodide; triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran / 3 h / 60 °C

2: piperidine / chloroform / 6 h / 60 °C

3: mercury dichloride / dimethyl sulfoxide; water / 3 h / 25 °C

With piperidine; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; mercury dichloride; In tetrahydrofuran; chloroform; water; dimethyl sulfoxide; 1: |Sonogashira Cross-Coupling;
DOI:10.1021/ol4000873