O-(2-acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-β-D-glucopyranosyl)-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-β-glucopyranosyl azide

Base Information

Chemical Name:O-(2-acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-β-D-glucopyranosyl)-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-β-glucopyranosyl azide
CAS No.:344597-16-6
Molecular Formula:C₄₄H₄₉N₅O₁₀
Molecular Weight:807.901
Hs Code.:

Synonyms:O-(2-acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-β-D-glucopyranosyl)-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-β-glucopyranosyl azide

Suppliers and Price of O-(2-acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-β-D-glucopyranosyl)-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-β-glucopyranosyl azide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of O-(2-acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-β-D-glucopyranosyl)-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-β-glucopyranosyl azide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of O-(2-acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-β-D-glucopyranosyl)-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-β-glucopyranosyl azide

There total 11 articles about O-(2-acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-β-D-glucopyranosyl)-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-β-glucopyranosyl azide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 10022-13-6
1,3,4,6-tetra-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranose

: 344597-16-6
O-(2-acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-β-D-glucopyranosyl)-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-β-glucopyranosyl azide

Guidance literature:: Multi-step reaction with 10 steps

1: NH₂NH₂; AcOH / dimethylformamide

2: imidazole; 4-dimethylaminopyridine / dimethylformamide

3: t-BuOK / methanol; tetrahydrofuran

4: camphorsulfonic acid / acetonitrile

5: NaH / dimethylformamide

6: tetrabutylammonium fluoride; AcOH / tetrahydrofuran

7: dimethylaminosulfur trifluoride / tetrahydrofuran

8: 81 percent / Cp₂HfCl₂; AgClO₄ / CH₂Cl₂

9: ethylenediamine / butan-1-ol

10: methanol

With 1H-imidazole; dmap; bis(cyclopentadienyl)hafnium dichloride; dimethylaminosulphur trifluoride; camphor-10-sulfonic acid; potassium tert-butylate; tetrabutyl ammonium fluoride; silver perchlorate; sodium hydride; acetic acid; ethylenediamine; hydrazine; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile; butan-1-ol;
DOI:10.1016/S0040-4039(01)00342-2

Reference yield:

: 72858-55-0
3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

: 344597-16-6
O-(2-acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-β-D-glucopyranosyl)-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-β-glucopyranosyl azide

Guidance literature:: Multi-step reaction with 9 steps

1: imidazole; 4-dimethylaminopyridine / dimethylformamide

2: t-BuOK / methanol; tetrahydrofuran

3: camphorsulfonic acid / acetonitrile

4: NaH / dimethylformamide

5: tetrabutylammonium fluoride; AcOH / tetrahydrofuran

6: dimethylaminosulfur trifluoride / tetrahydrofuran

7: 81 percent / Cp₂HfCl₂; AgClO₄ / CH₂Cl₂

8: ethylenediamine / butan-1-ol

9: methanol

With 1H-imidazole; dmap; bis(cyclopentadienyl)hafnium dichloride; dimethylaminosulphur trifluoride; camphor-10-sulfonic acid; potassium tert-butylate; tetrabutyl ammonium fluoride; silver perchlorate; sodium hydride; acetic acid; ethylenediamine; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile; butan-1-ol;
DOI:10.1016/S0040-4039(01)00342-2

Reference yield:

: 277310-81-3
3-O-benzyl-4,6-O-benzylidene-2-deoxy-2-phthalimido-β-D-glucopyranosyl fluoride

: 344597-16-6
O-(2-acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-β-D-glucopyranosyl)-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-β-glucopyranosyl azide

Guidance literature:: Multi-step reaction with 3 steps

1: 81 percent / Cp₂HfCl₂; AgClO₄ / CH₂Cl₂

2: ethylenediamine / butan-1-ol

3: methanol

With bis(cyclopentadienyl)hafnium dichloride; silver perchlorate; ethylenediamine; In methanol; dichloromethane; butan-1-ol;
DOI:10.1016/S0040-4039(01)00342-2