Lupinine, (+)-

Base Information

Chemical Name:Lupinine, (+)-
CAS No.:7635-60-1
Molecular Formula:C₁₀H₁₉NO
Molecular Weight:169.267
Hs Code.:
UNII:0T273WHX1G
Nikkaji Number:J37.653A
Wikidata:Q27237215

Synonyms:Lupinine, (+)-;(+)-Lupinine;7635-60-1;2H-Quinolizine-1-methanol, octahydro-, (1S-trans)-;0T273WHX1G;2H-Quinolizine-1-methanol, octahydro-, (1S,9aS)-;((1S,9AS)-octahydro-2H-quinolizin-1-yl)methanol;1alphaH,10alpha-Lupinine;UNII-0T273WHX1G;Octahydro-2H-quinolizin-1-ylmethanol #;starbld0005351;2H-Quinolizine-1-methanol, octahydro-, (1R-trans)-;HDVAWXXJVMJBAR-ZJUUUORDSA-N;TNP00032;[(1S,9aS)-2,3,4,6,7,8,9,9a-octahydro-1H-quinolizin-1-yl]methanol;AKOS040752753;1.ALPHA.H,10.ALPHA.-LUPININE;NCGC00017172-01;Q27237215

Suppliers and Price of Lupinine, (+)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of Lupinine, (+)-

Chemical Property:

XLogP3:1.2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:169.146664230
Heavy Atom Count:12
Complexity:149

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1CCN2CCCC(C2C1)CO
Isomeric SMILES:C1CCN2CCC[C@@H]([C@@H]2C1)CO

Technology Process of Lupinine, (+)-

There total 6 articles about Lupinine, (+)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 753452-08-3
(3R,4R)-N-allyl-N-[(3-benzoxymethyl)-1,6-heptadien-4-yl]propenamide

: 7635-60-1
(+)-(1S,9aS)-1-(octahydro-quinolizin-1-yl)-methanol

: 486-70-4
lupinine

Guidance literature:: (3R,4R)-N-allyl-N-[(3-benzoxymethyl)-1,6-heptadien-4-yl]propenamide; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In dichloromethane; for 6h; Heating;

With hydrogen; acetic acid; palladium on activated charcoal; In methanol; at 30 ℃; for 24h; under 760 Torr;

With lithium aluminium tetrahydride; In tetrahydrofuran; for 4h; Title compound not separated from byproducts; Heating;
DOI:10.1002/chem.200305581

Reference yield:

: 753452-09-4
(3S,4S)-N-allyl-N-[(3-benzoxymethyl)-1,6-heptadien-4-yl]propenamide

: 7635-60-1
(+)-(1S,9aS)-1-(octahydro-quinolizin-1-yl)-methanol

: 486-70-4
lupinine

Guidance literature:: (3S,4S)-N-allyl-N-[(3-benzoxymethyl)-1,6-heptadien-4-yl]propenamide; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In dichloromethane; for 6h; Heating;

With hydrogen; acetic acid; palladium on activated charcoal; In methanol; at 30 ℃; for 24h; under 760 Torr;

With lithium aluminium tetrahydride; In tetrahydrofuran; for 4h; Title compound not separated from byproducts; Heating;
DOI:10.1002/chem.200305581