(E)-S-2-acetamidoethyl 3-{4-[(E)-3,7-dimethylocta-2,6-dienyloxy]-phenyl}prop-2-enethioate

Base Information

Chemical Name:(E)-S-2-acetamidoethyl 3-{4-[(E)-3,7-dimethylocta-2,6-dienyloxy]-phenyl}prop-2-enethioate
CAS No.:1119760-57-4
Molecular Formula:C₂₃H₃₁NO₃S
Molecular Weight:401.57
Hs Code.:

Synonyms:(E)-S-2-acetamidoethyl 3-{4-[(E)-3,7-dimethylocta-2,6-dienyloxy]-phenyl}prop-2-enethioate

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Chemical Property of (E)-S-2-acetamidoethyl 3-{4-[(E)-3,7-dimethylocta-2,6-dienyloxy]-phenyl}prop-2-enethioate

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Technology Process of (E)-S-2-acetamidoethyl 3-{4-[(E)-3,7-dimethylocta-2,6-dienyloxy]-phenyl}prop-2-enethioate

There total 4 articles about (E)-S-2-acetamidoethyl 3-{4-[(E)-3,7-dimethylocta-2,6-dienyloxy]-phenyl}prop-2-enethioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: Geranyloxy-p-coumaric acid

: 1190-73-4
2-(acetylamino)ethanethiol

: 1119760-57-4
(E)-S-2-acetamidoethyl 3-{4-[(E)-3,7-dimethylocta-2,6-dienyloxy]-phenyl}prop-2-enethioate

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1021/jm101510d

Reference yield:

: 3943-97-3
methyl 4-hydroxycinnamate

: 1119760-57-4
(E)-S-2-acetamidoethyl 3-{4-[(E)-3,7-dimethylocta-2,6-dienyloxy]-phenyl}prop-2-enethioate

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate; potassium iodide / acetone / 20 h / Reflux

2: water; potassium carbonate / methanol / 3 h / Reflux

3: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 24 h / 20 °C / Inert atmosphere

With dmap; water; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; potassium iodide; In methanol; dichloromethane; acetone;
DOI:10.1021/jm101510d

Reference yield:

: 7400-08-0,50940-26-6
p-Coumaric Acid

: 1119760-57-4
(E)-S-2-acetamidoethyl 3-{4-[(E)-3,7-dimethylocta-2,6-dienyloxy]-phenyl}prop-2-enethioate

Guidance literature:: Multi-step reaction with 4 steps

1: sulfuric acid / 24 h / Molecular sieve

2: potassium carbonate; potassium iodide / acetone / 20 h / Reflux

3: water; potassium carbonate / methanol / 3 h / Reflux

4: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 24 h / 20 °C / Inert atmosphere

With dmap; sulfuric acid; water; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; potassium iodide; In methanol; dichloromethane; acetone;
DOI:10.1021/jm101510d