tert-Butyl-{(S)-2-methoxymethoxy-2-[(2R,5R,2'R,5'R)-5'-((R)-1-methoxymethoxy-undecyl)-octahydro-[2,2']bifuranyl-5-yl]-ethoxy}-diphenyl-silane

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Chemical Name:tert-Butyl-{(S)-2-methoxymethoxy-2-[(2R,5R,2'R,5'R)-5'-((R)-1-methoxymethoxy-undecyl)-octahydro-[2,2']bifuranyl-5-yl]-ethoxy}-diphenyl-silane
CAS No.:165961-18-2
Molecular Formula:C₄₁H₆₆O₇Si
Molecular Weight:699.056
Hs Code.:

Synonyms:tert-Butyl-{(S)-2-methoxymethoxy-2-[(2R,5R,2'R,5'R)-5'-((R)-1-methoxymethoxy-undecyl)-octahydro-[2,2']bifuranyl-5-yl]-ethoxy}-diphenyl-silane

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Chemical Property of tert-Butyl-{(S)-2-methoxymethoxy-2-[(2R,5R,2'R,5'R)-5'-((R)-1-methoxymethoxy-undecyl)-octahydro-[2,2']bifuranyl-5-yl]-ethoxy}-diphenyl-silane

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Technology Process of tert-Butyl-{(S)-2-methoxymethoxy-2-[(2R,5R,2'R,5'R)-5'-((R)-1-methoxymethoxy-undecyl)-octahydro-[2,2']bifuranyl-5-yl]-ethoxy}-diphenyl-silane

There total 10 articles about tert-Butyl-{(S)-2-methoxymethoxy-2-[(2R,5R,2'R,5'R)-5'-((R)-1-methoxymethoxy-undecyl)-octahydro-[2,2']bifuranyl-5-yl]-ethoxy}-diphenyl-silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 107-30-2
chloromethyl methyl ether

: 165961-17-1
(+)-(2S,3R,6R,7R,10R,11R)-1-O-(tert-Butyldiphenylsilyl)-2-O-(methoxymethyl)-3,6:7,10-diepoxy-1,2,11-trihydroxyhenicosane

: 165961-18-2
tert-Butyl-{(S)-2-methoxymethoxy-2-[(2R,5R,2'R,5'R)-5'-((R)-1-methoxymethoxy-undecyl)-octahydro-[2,2']bifuranyl-5-yl]-ethoxy}-diphenyl-silane

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; for 12h; Ambient temperature;
DOI:10.1021/jo00119a019

Reference yield:

: 39691-62-8
nonylmagnesium bromide

: 165961-18-2
tert-Butyl-{(S)-2-methoxymethoxy-2-[(2R,5R,2'R,5'R)-5'-((R)-1-methoxymethoxy-undecyl)-octahydro-[2,2']bifuranyl-5-yl]-ethoxy}-diphenyl-silane

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / CuBr / tetrahydrofuran / 1 h / 0 °C

2: 98 percent / i-Pr₂NEt / CH₂Cl₂ / 12 h / Ambient temperature

With N-ethyl-N,N-diisopropylamine; copper(I) bromide; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo00119a019

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 165961-18-2
tert-Butyl-{(S)-2-methoxymethoxy-2-[(2R,5R,2'R,5'R)-5'-((R)-1-methoxymethoxy-undecyl)-octahydro-[2,2']bifuranyl-5-yl]-ethoxy}-diphenyl-silane

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / Et₃N, imidazole / CH₂Cl₂ / 1.5 h / Ambient temperature

2: 87 percent / CuBr / tetrahydrofuran / 1 h / 0 °C

3: 98 percent / i-Pr₂NEt / CH₂Cl₂ / 12 h / Ambient temperature

With 1H-imidazole; triethylamine; N-ethyl-N,N-diisopropylamine; copper(I) bromide; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo00119a019