methyl 7-[4-(2-propoxyethoxy)phenyl]-1-propyl-2,3-dihydro-1-benzazepine-4-carbonate

Base Information

Chemical Name:methyl 7-[4-(2-propoxyethoxy)phenyl]-1-propyl-2,3-dihydro-1-benzazepine-4-carbonate
CAS No.:497855-99-9
Molecular Formula:C₂₆H₃₃NO₄
Molecular Weight:423.552
Hs Code.:

Synonyms:methyl 7-[4-(2-propoxyethoxy)phenyl]-1-propyl-2,3-dihydro-1-benzazepine-4-carbonate

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Chemical Property of methyl 7-[4-(2-propoxyethoxy)phenyl]-1-propyl-2,3-dihydro-1-benzazepine-4-carbonate

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Technology Process of methyl 7-[4-(2-propoxyethoxy)phenyl]-1-propyl-2,3-dihydro-1-benzazepine-4-carbonate

There total 1 articles about methyl 7-[4-(2-propoxyethoxy)phenyl]-1-propyl-2,3-dihydro-1-benzazepine-4-carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 497856-41-4
methyl 7-bromo-1-propyl-2,3-dihydro-1H-1-benzazepine-4-carboxylate

: 279262-27-0
{4-[2-(propoxy)ethoxy]phenyl}boronic acid

: 497855-99-9
methyl 7-[4-(2-propoxyethoxy)phenyl]-1-propyl-2,3-dihydro-1-benzazepine-4-carbonate

Guidance literature:: methyl 7-bromo-1-propyl-2,3-dihydro-1H-1-benzazepine-4-carboxylate; {4-[2-(propoxy)ethoxy]phenyl}boronic acid; With potassium carbonate; In ethanol; water; toluene; for 1h;

tetrakis(triphenylphosphine) palladium⁽⁰⁾; In ethanol; water; toluene; for 2h; Heating / reflux;

Reference yield:

: 497855-99-9
methyl 7-[4-(2-propoxyethoxy)phenyl]-1-propyl-2,3-dihydro-1-benzazepine-4-carbonate

: 497851-61-3
7-[4-(2-propoxyethoxy)phenyl]-1-propyl-2,3-dihydro-1-benzazepine-4-carboxylic acid

Guidance literature:: methyl 7-[4-(2-propoxyethoxy)phenyl]-1-propyl-2,3-dihydro-1-benzazepine-4-carbonate; With sodium hydroxide; In tetrahydrofuran; methanol; water; at 0 - 60 ℃;

With hydrogenchloride; In tetrahydrofuran; methanol; water; at 0 ℃;