2,5-bis(2-ethylhexyl)-3,6-bis(5-(p-tolyl)thiophen-2-yl)pyrrolo[3,4-c]pyrrole-1,4(2H,5H)-dione

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Chemical Name:2,5-bis(2-ethylhexyl)-3,6-bis(5-(p-tolyl)thiophen-2-yl)pyrrolo[3,4-c]pyrrole-1,4(2H,5H)-dione
CAS No.:1423186-21-3
Molecular Formula:C₄₄H₅₂N₂O₂S₂
Molecular Weight:705.041
Hs Code.:

Synonyms:2,5-bis(2-ethylhexyl)-3,6-bis(5-(p-tolyl)thiophen-2-yl)pyrrolo[3,4-c]pyrrole-1,4(2H,5H)-dione

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Chemical Property of 2,5-bis(2-ethylhexyl)-3,6-bis(5-(p-tolyl)thiophen-2-yl)pyrrolo[3,4-c]pyrrole-1,4(2H,5H)-dione

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Technology Process of 2,5-bis(2-ethylhexyl)-3,6-bis(5-(p-tolyl)thiophen-2-yl)pyrrolo[3,4-c]pyrrole-1,4(2H,5H)-dione

There total 2 articles about 2,5-bis(2-ethylhexyl)-3,6-bis(5-(p-tolyl)thiophen-2-yl)pyrrolo[3,4-c]pyrrole-1,4(2H,5H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1185885-86-2
2,5-bis(2-ethylhexyl)-3,6-di(thiophen-2-yl)pyrrolo[3,4-c]pyrrole-1,4-dione

: 106-38-7
para-bromotoluene

: 1423186-21-3
2,5-bis(2-ethylhexyl)-3,6-bis(5-(p-tolyl)thiophen-2-yl)pyrrolo[3,4-c]pyrrole-1,4(2H,5H)-dione

Guidance literature:: With palladium diacetate; potassium carbonate; Trimethylacetic acid; In N,N-dimethyl acetamide; at 110 ℃; for 4h; Inert atmosphere; Schlenk technique;
DOI:10.1039/c2ta01318e

Reference yield: 69.0%

: 1185885-86-2
2,5-bis(2-ethylhexyl)-3,6-di(thiophen-2-yl)pyrrolo[3,4-c]pyrrole-1,4-dione

: 624-31-7
4-tolyl iodide

: 1423186-21-3
2,5-bis(2-ethylhexyl)-3,6-bis(5-(p-tolyl)thiophen-2-yl)pyrrolo[3,4-c]pyrrole-1,4(2H,5H)-dione

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tris(o-methoxyphenyl)phosphine; caesium carbonate; Trimethylacetic acid; In neat (no solvent); at 110 ℃; for 15h; Schlenk technique; Sealed tube; Green chemistry;
DOI:10.1021/acs.joc.8b01284