(E)-10-phenyldec-9-en-3-yn-2-one

Base Information

Chemical Name:(E)-10-phenyldec-9-en-3-yn-2-one
CAS No.:1395054-15-5
Molecular Formula:C₁₆H₁₈O
Molecular Weight:226.318
Hs Code.:

Synonyms:(E)-10-phenyldec-9-en-3-yn-2-one

Suppliers and Price of (E)-10-phenyldec-9-en-3-yn-2-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-10-phenyldec-9-en-3-yn-2-one

Chemical Property:

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Technology Process of (E)-10-phenyldec-9-en-3-yn-2-one

There total 5 articles about (E)-10-phenyldec-9-en-3-yn-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 127-19-5,116057-81-9
N,N-dimethyl acetamide

: 1395054-36-0
(E)-oct-1-en-7-yn-1-ylbenzene

: 1395054-15-5
(E)-10-phenyldec-9-en-3-yn-2-one

Guidance literature:: (E)-oct-1-en-7-yn-1-ylbenzene; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.75h;

N,N-dimethyl acetamide; In tetrahydrofuran; hexane; for 0.0833333h;

With boron trifluoride diethyl etherate; acetic acid; In tetrahydrofuran; hexane; at -78 - -20 ℃;
DOI:10.1021/ol301938z

Reference yield: 68.0%

: 1395054-15-5
(E)-10-phenyldec-9-en-3-yn-2-one

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; for 0.75h; Cooling with acetone-dry ice; Inert atmosphere;

With boron trifluoride diethyl etherate; In tetrahydrofuran; hexane; Cooling with acetone-dry ice;

With boron trifluoride diethyl etherate; acetic acid; In tetrahydrofuran; hexane; Cooling with acetone-dry ice;

Reference yield:

: 63478-76-2
1-hydroxy-6-heptyne

: 1395054-15-5
(E)-10-phenyldec-9-en-3-yn-2-one

Guidance literature:: Multi-step reaction with 3 steps

1.1: pyridinium chlorochromate / dichloromethane / 3.5 h / 20 °C

2.1: sodium hydride / mineral oil; tetrahydrofuran / 0.33 h / 20 °C / Inert atmosphere

2.2: 4.08 h / Inert atmosphere; Reflux

3.1: n-butyllithium / tetrahydrofuran; hexane / 0.75 h / -78 °C

3.2: 0.08 h

3.3: -78 - -20 °C

With n-butyllithium; sodium hydride; pyridinium chlorochromate; In tetrahydrofuran; hexane; dichloromethane; mineral oil;
DOI:10.1021/ol301938z