N,N',N'',N'''-tetrakis(o-nitrobenzenesulfonyl)-1,5,8,12-tetraazadodecane

Base Information

Chemical Name:N,N',N'',N'''-tetrakis(o-nitrobenzenesulfonyl)-1,5,8,12-tetraazadodecane
CAS No.:210303-87-0
Molecular Formula:C₃₂H₃₄N₈O₁₆S₄
Molecular Weight:914.93
Hs Code.:

Synonyms:N,N',N'',N'''-tetrakis(o-nitrobenzenesulfonyl)-1,5,8,12-tetraazadodecane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N',N'',N'''-tetrakis(o-nitrobenzenesulfonyl)-1,5,8,12-tetraazadodecane

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Technology Process of N,N',N'',N'''-tetrakis(o-nitrobenzenesulfonyl)-1,5,8,12-tetraazadodecane

There total 1 articles about N,N',N'',N'''-tetrakis(o-nitrobenzenesulfonyl)-1,5,8,12-tetraazadodecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 10563-26-5
N,N'-bis(3-aminopropyl)-1,2-diamine

: 1694-92-4
2-Nitrobenzenesulfonyl chloride

: 210303-87-0
N,N',N'',N'''-tetrakis(o-nitrobenzenesulfonyl)-1,5,8,12-tetraazadodecane

Guidance literature:: With triethylamine; In dichloromethane; for 30h;
DOI:10.1016/S0040-4039(98)00587-5

Reference yield: 98.0%

: 58791-49-4
1,4-bis(bromomethyl)naphthalene

: 210303-87-0
N,N',N'',N'''-tetrakis(o-nitrobenzenesulfonyl)-1,5,8,12-tetraazadodecane

: N,N',N'',N'''-tetrakis(o-nitrobenzenesulfonyl)-2,6,9,13-tetraaza[14](1,4)naphthalenophane

Guidance literature:: With potassium carbonate; In acetonitrile; Heating;
DOI:10.1016/S0040-4039(98)00587-5

Reference yield: 28.0%

: 58791-49-4
1,4-bis(bromomethyl)naphthalene

: 210303-87-0
N,N',N'',N'''-tetrakis(o-nitrobenzenesulfonyl)-1,5,8,12-tetraazadodecane

: 2,6,9,13-tetraaza[14](1,4)naphthalenophane hydrochloride

Guidance literature:: 1,4-bis(bromomethyl)naphthalene; N,N',N'',N'''-tetrakis(o-nitrobenzenesulfonyl)-1,5,8,12-tetraazadodecane; With potassium carbonate; In N,N-dimethyl-formamide; at 90 ℃; for 72h;

With 2-hydroxyethanethiol; In N,N-dimethyl-formamide; at 20 ℃; for 15h;

With hydrogenchloride; In methanol;
DOI:10.1016/S0040-4020(02)00180-1