1,2-Diazido-4-methylcyclohexane

Base Information

• Chemical Name: 1,2-Diazido-4-methylcyclohexane
• CAS No.: 1246967-35-0
• Molecular Formula: C₇H₁₂N₆
• Molecular Weight: 180.212
• DSSTox Substance ID: DTXSID101303537
• Mol file: 1246967-35-0.mol

Synonyms:1,2-diazido-4-methylcyclohexane;DTXSID101303537;1246967-35-0

Chemical Property of 1,2-Diazido-4-methylcyclohexane

Chemical Property:

• XLogP3: 3.7
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 2
• Exact Mass: 180.11234441
• Heavy Atom Count: 13
• Complexity: 262

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: CC1CCC(C(C1)N=[N+]=[N-])N=[N+]=[N-]

Technology Process of 1,2-Diazido-4-methylcyclohexane

There total 1 articles about 1,2-Diazido-4-methylcyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-methylcyclohexene (591-47-9) → 4-methyl-trans-(+/-)-1,2-diazidocyclohexane (1246967-35-0)

Guidance literature:

With sodium azide; trifluoroacetic acid; In acetonitrile; at -21 - -19 ℃; for 3h;

DOI:10.1016/j.tet.2007.10.069

Reference yield:

4-methyl-trans-(+/-)-1,2-diazidocyclohexane (1246967-35-0) → 4-methyl-trans-(+/-)-1,2-cyclohexanediamine (636563-62-7,758705-57-6,761426-11-3,761427-52-5) + 4-methyl-trans-(+/-)-1,2-cyclohexanediamine (636563-62-7,758705-57-6,761426-11-3,761427-52-5)

Guidance literature:

With hydrogen; Lindlar's catalyst; In ethanol; for 24h; under 2250.23 Torr; Title compound not separated from byproducts.;

DOI:10.1016/j.tet.2007.10.069

upstream raw materials:

4-methylcyclohexene

Downstream raw materials:

4-methyl-trans-(+/-)-1,2-cyclohexanediamine

4-methyl-trans-(+/-)-1,2-cyclohexanediamine