1-benzyl-2-(naphthalen-2-yl)disulfide

Base Information

• Chemical Name: 1-benzyl-2-(naphthalen-2-yl)disulfide
• CAS No.: 15515-57-8
• Molecular Formula: C₁₇H₁₄S₂
• Molecular Weight: 282.43
• Mol file: 15515-57-8.mol

Synonyms:1-benzyl-2-(naphthalen-2-yl)disulfide

Chemical Property of 1-benzyl-2-(naphthalen-2-yl)disulfide

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 1-benzyl-2-(naphthalen-2-yl)disulfide

There total 10 articles about 1-benzyl-2-(naphthalen-2-yl)disulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

C13H12OS2 + benzyl thiosulphate (6313-36-6) → 1-benzyl-2-(naphthalen-2-yl)disulfide (15515-57-8)

Guidance literature:

With potassium carbonate; at 80 ℃; for 12h;

DOI:10.1055/s-0037-1609081

Reference yield: 78.0%

sodium naphthalen-2-ylsulfinate (63735-42-2) + benzyl chloride (100-44-7) → 1-benzyl-2-(naphthalen-2-yl)disulfide (15515-57-8)

Guidance literature:

benzyl chloride; With Sodium thiosulfate pentahydrate; In ethanol; water; at 100 ℃; for 2h; Inert atmosphere;

sodium naphthalen-2-ylsulfinate; In 1,4-dioxane; at 110 ℃; for 11h; Inert atmosphere;

Reference yield: 78.0%

2-(benzylsulfinothioyl)isoindoline-1,3-dione (33704-38-0) + naphthalene-2-boronic acid (32316-92-0) → 1-benzyl-2-(naphthalen-2-yl)disulfide (15515-57-8)

Guidance literature:

With [2,2]bipyridinyl; potassium phosphate; copper diacetate; In tetrahydrofuran; water; at 40 ℃; for 10h; Inert atmosphere;

DOI:10.1021/acscatal.9b04326

upstream raw materials:

benzyl triphenylmethyl sulfide

2-naphthalenesulfenyl thiocyanate

phenylmethanethiol

2-Naphthalenethiol