C₂₄H₃₀O₄Si

Base Information

Chemical Name:C₂₄H₃₀O₄Si
CAS No.:1612775-35-5
Molecular Formula:C₂₄H₃₀O₄Si
Molecular Weight:410.585
Hs Code.:

C<sub>24</sub>H<sub>30</sub>O<sub>4</sub>Si

Synonyms:C₂₄H₃₀O₄Si

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Chemical Property of C₂₄H₃₀O₄Si

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Technology Process of C₂₄H₃₀O₄Si

There total 3 articles about C₂₄H₃₀O₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1612775-34-4
C₃₁H₃₄O₆SSi

: 1612775-35-5
C₂₄H₃₀O₄Si

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In toluene; for 0.5h; Inert atmosphere; Reflux;
DOI:10.1021/ol501446w

Reference yield:

: C₂₄H₃₂O₅Si

: 1612775-35-5
C₂₄H₃₀O₄Si

Guidance literature:: Multi-step reaction with 3 steps

1: N-iodo-succinimide; tetra-(n-butyl)ammonium iodide / dichloromethane / 21 h / 20 °C / Inert atmosphere

2: dmap / acetonitrile / 0.67 h / 0 °C / Inert atmosphere

3: tri-n-butyl-tin hydride; 2,2'-azobis(isobutyronitrile) / toluene / 0.5 h / Inert atmosphere; Reflux

With dmap; N-iodo-succinimide; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; tetra-(n-butyl)ammonium iodide; In dichloromethane; toluene; acetonitrile; 3: |Barton-McCombie Deoxygenation;
DOI:10.1021/ol501446w

Reference yield:

: 1612775-33-3
C₂₄H₃₀O₅Si

: 1612775-35-5
C₂₄H₃₀O₄Si

Guidance literature:: Multi-step reaction with 2 steps

1: dmap / acetonitrile / 0.67 h / 0 °C / Inert atmosphere

2: tri-n-butyl-tin hydride; 2,2'-azobis(isobutyronitrile) / toluene / 0.5 h / Inert atmosphere; Reflux

With dmap; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In toluene; acetonitrile; 2: |Barton-McCombie Deoxygenation;
DOI:10.1021/ol501446w