(M)-(-)-2,7,12-trimethoxy-3,8,13-tris<(2-phenyltetrazolyl)oxy>-10,15-dihydro-5H-tribenzocyclononene

Base Information

Chemical Name:(M)-(-)-2,7,12-trimethoxy-3,8,13-tris<(2-phenyltetrazolyl)oxy>-10,15-dihydro-5H-tribenzocyclononene
CAS No.:89255-58-3
Molecular Formula:C₄₅H₃₆N₁₂O₆
Molecular Weight:840.858
Hs Code.:

(M)-(-)-2,7,12-trimethoxy-3,8,13-tris<(2-phenyltetrazolyl)oxy>-10,15-dihydro-5H-tribenzo<a,d,g>cyclononene

Synonyms:(M)-(-)-2,7,12-trimethoxy-3,8,13-tris<(2-phenyltetrazolyl)oxy>-10,15-dihydro-5H-tribenzocyclononene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (M)-(-)-2,7,12-trimethoxy-3,8,13-tris<(2-phenyltetrazolyl)oxy>-10,15-dihydro-5H-tribenzocyclononene

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Technology Process of (M)-(-)-2,7,12-trimethoxy-3,8,13-tris<(2-phenyltetrazolyl)oxy>-10,15-dihydro-5H-tribenzocyclononene

There total 2 articles about (M)-(-)-2,7,12-trimethoxy-3,8,13-tris<(2-phenyltetrazolyl)oxy>-10,15-dihydro-5H-tribenzocyclononene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 14210-25-4
5-Chloro-1-phenyltetrazole

: 68182-93-4
(P)-(-)-2,7,12-trihydroxy-3,8,13-trimethoxy-10,15-dihydro-5H-tribenzocyclononene <(-)-C₃-cyclotriguaiacylene>

: 89255-58-3
(M)-(-)-2,7,12-trimethoxy-3,8,13-tris<(2-phenyltetrazolyl)oxy>-10,15-dihydro-5H-tribenzocyclononene

Guidance literature:: With potassium tert-butylate; In N,N-dimethyl-formamide; 1) 10 min, 2) 1 h;
DOI:10.1021/ja00332a042

Reference yield:

: C₅₄H₆₀O₁₅

: 89255-58-3
(M)-(-)-2,7,12-trimethoxy-3,8,13-tris<(2-phenyltetrazolyl)oxy>-10,15-dihydro-5H-tribenzocyclononene

Guidance literature:: Multi-step reaction with 2 steps

1: LiAlH₄ / 0 °C

2: 1) tert-BuOK / dimethylformamide / 1) 10 min, 2) 1 h

With lithium aluminium tetrahydride; potassium tert-butylate; In N,N-dimethyl-formamide;
DOI:10.1021/ja00332a042