tert-butyl {4-[(E)-2-(6-bromopyridin-3-yl)vinyl]phenyl}methyl-carbamate

Base Information

Chemical Name:tert-butyl {4-[(E)-2-(6-bromopyridin-3-yl)vinyl]phenyl}methyl-carbamate
CAS No.:1349698-22-1
Molecular Formula:C₁₉H₂₁BrN₂O₂
Molecular Weight:389.292
Hs Code.:

Synonyms:tert-butyl {4-[(E)-2-(6-bromopyridin-3-yl)vinyl]phenyl}methyl-carbamate

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Chemical Property of tert-butyl {4-[(E)-2-(6-bromopyridin-3-yl)vinyl]phenyl}methyl-carbamate

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Technology Process of tert-butyl {4-[(E)-2-(6-bromopyridin-3-yl)vinyl]phenyl}methyl-carbamate

There total 5 articles about tert-butyl {4-[(E)-2-(6-bromopyridin-3-yl)vinyl]phenyl}methyl-carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.6%

: 73290-22-9
2-bromo-5-iodo-pyridine

: 937183-61-4
4-N-(tert-butyloxycarbonyl)-4-N-methylaminostyrene

: 1349698-22-1
tert-butyl {4-[(E)-2-(6-bromopyridin-3-yl)vinyl]phenyl}methyl-carbamate

Guidance literature:: With tetrabutylammomium bromide; palladium diacetate; potassium carbonate; In N,N-dimethyl-formamide; at 65 ℃; for 3h; Reagent/catalyst; Inert atmosphere;

Reference yield:

: 193204-58-9
tert-butyl N-(4-{2-[(4-methylbenzenesulfonyl)oxy]ethyl}phenyl)carbamate

: 1349698-22-1
tert-butyl {4-[(E)-2-(6-bromopyridin-3-yl)vinyl]phenyl}methyl-carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 - 20 °C / Inert atmosphere

2: tetrabutylammomium bromide; potassium carbonate; palladium diacetate / N,N-dimethyl-formamide / 3 h / 65 °C / Inert atmosphere

With tetrabutylammomium bromide; palladium diacetate; sodium hydride; potassium carbonate; In N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 2-[4-(tert-butoxycarbonylamino)phenyl]ethylmethanesulfonate

: 1349698-22-1
tert-butyl {4-[(E)-2-(6-bromopyridin-3-yl)vinyl]phenyl}methyl-carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 - 20 °C / Inert atmosphere

2: tetrabutylammomium bromide; potassium carbonate; palladium diacetate / N,N-dimethyl-formamide / 3 h / 65 °C / Inert atmosphere

With tetrabutylammomium bromide; palladium diacetate; sodium hydride; potassium carbonate; In N,N-dimethyl-formamide; mineral oil;