1-N-(p-nitrobenzoyl)-D,L-phenylalanyl-4-(p-bromophenyl)thiosemicarbazide

Base Information

• Chemical Name: 1-N-(p-nitrobenzoyl)-D,L-phenylalanyl-4-(p-bromophenyl)thiosemicarbazide
• CAS No.: 1198464-65-1
• Molecular Formula: C₂₃H₂₀BrN₅O₄S
• Molecular Weight: 542.413

Synonyms:1-N-(p-nitrobenzoyl)-D,L-phenylalanyl-4-(p-bromophenyl)thiosemicarbazide

Chemical Property of 1-N-(p-nitrobenzoyl)-D,L-phenylalanyl-4-(p-bromophenyl)thiosemicarbazide

Chemical Property:

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Technology Process of 1-N-(p-nitrobenzoyl)-D,L-phenylalanyl-4-(p-bromophenyl)thiosemicarbazide

There total 1 articles about 1-N-(p-nitrobenzoyl)-D,L-phenylalanyl-4-(p-bromophenyl)thiosemicarbazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.33%

N-(p-nitrobenzoyl)-D,L-phenylalanine hydrazide (1198464-64-0) + 4-Bromophenyl isothiocyanate (1985-12-2) → 1-N-(p-nitrobenzoyl)-D,L-phenylalanyl-4-(p-bromophenyl)thiosemicarbazide (1198464-65-1)

Guidance literature:

In methanol; at 70 - 80 ℃; for 3h;

DOI:10.3390/molecules14072621

Reference yield: 71.5%

1-N-(p-nitrobenzoyl)-D,L-phenylalanyl-4-(p-bromophenyl)thiosemicarbazide (1198464-65-1) → 2-[1-(p-nitrobenzoylamino)-2-phenyl]ethyl-5-(p-bromophenylamino)-1,3,4-thiadiazole (1198464-67-3)

Guidance literature:

With sulfuric acid; at 20 ℃; for 1h;

DOI:10.3390/molecules14072621

Reference yield: 64.45%

1-N-(p-nitrobenzoyl)-D,L-phenylalanyl-4-(p-bromophenyl)thiosemicarbazide (1198464-65-1) → 4-(p-bromophenyl)-5-[1-(p-nitrobenzoylamino)-2-phenylethyl]-3-thio-1,2,4-triazole (1198464-69-5)

Guidance literature:

With sodium hydroxide; In water; at 80 - 90 ℃; for 4h;

DOI:10.3390/molecules14072621

upstream raw materials:

N-(p-nitrobenzoyl)-D,L-phenylalanine hydrazide

4-Bromophenyl isothiocyanate

Downstream raw materials:

2-[1-(p-nitrobenzoylamino)-2-phenyl]ethyl-5-(p-bromophenylamino)-1,3,4-thiadiazole

4-(p-bromophenyl)-5-[1-(p-nitrobenzoylamino)-2-phenylethyl]-3-thio-1,2,4-triazole

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