2-endo-(phenylamino)-4-endo-hydroxyprotoadamantane

Base Information

Chemical Name:2-endo-(phenylamino)-4-endo-hydroxyprotoadamantane
CAS No.:83863-00-7
Molecular Formula:C₁₆H₂₁NO
Molecular Weight:243.349
Hs Code.:

Synonyms:2-endo-(phenylamino)-4-endo-hydroxyprotoadamantane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-endo-(phenylamino)-4-endo-hydroxyprotoadamantane

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Technology Process of 2-endo-(phenylamino)-4-endo-hydroxyprotoadamantane

There total 3 articles about 2-endo-(phenylamino)-4-endo-hydroxyprotoadamantane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 83862-94-6
N-phenyl-4,2-(epoxyimino)protoadamantane

: 83863-00-7
2-endo-(phenylamino)-4-endo-hydroxyprotoadamantane

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 3h; Ambient temperature;
DOI:10.1021/jo00148a005

Reference yield:

: 23014-71-3,65437-67-4
4-oxotricyclo [3.3.1.1^{3, 7}]dec-2-yl methanesulfonate

: 83863-00-7
2-endo-(phenylamino)-4-endo-hydroxyprotoadamantane

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) NaBH₄, 2.) 1percent aq. NaHCO₃ / 1.) MeOH, H₂O, -10 to -15 deg C, 2 h, 2.) ether, reflux, 2 h

2: 23 percent / molecular sieve (4A or 3A) / dimethylsulfoxide / 20 h / 20 - 25 °C

3: 58 percent / H₂ / 10percent Pd/C / methanol / 3 h / Ambient temperature

With sodium tetrahydroborate; 3 A molecular sieve; hydrogen; sodium hydrogencarbonate; palladium on activated charcoal; In methanol; dimethyl sulfoxide;
DOI:10.1021/jo00148a005

Reference yield:

: 31603-46-0
endo-bicyclo<3.3.1>non-6-ene-3-carboxaldehyde

: 83863-00-7
2-endo-(phenylamino)-4-endo-hydroxyprotoadamantane

Guidance literature:: Multi-step reaction with 2 steps

1: 23 percent / molecular sieve (4A or 3A) / dimethylsulfoxide / 20 h / 20 - 25 °C

2: 58 percent / H₂ / 10percent Pd/C / methanol / 3 h / Ambient temperature

With 3 A molecular sieve; hydrogen; palladium on activated charcoal; In methanol; dimethyl sulfoxide;
DOI:10.1021/jo00148a005