1-chloro-1-(3-bromophenyl)-5,9-dimethyl-5,9-undecadiene

Base Information

Chemical Name:1-chloro-1-(3-bromophenyl)-5,9-dimethyl-5,9-undecadiene
CAS No.:205117-90-4
Molecular Formula:C₁₉H₂₆BrCl
Molecular Weight:369.772
Hs Code.:

Synonyms:1-chloro-1-(3-bromophenyl)-5,9-dimethyl-5,9-undecadiene

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Chemical Property of 1-chloro-1-(3-bromophenyl)-5,9-dimethyl-5,9-undecadiene

Chemical Property:

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Technology Process of 1-chloro-1-(3-bromophenyl)-5,9-dimethyl-5,9-undecadiene

There total 3 articles about 1-chloro-1-(3-bromophenyl)-5,9-dimethyl-5,9-undecadiene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1-(3-bromophenyl)-5,9-dimethyl-5,9-undecadienol

: 205117-90-4
1-chloro-1-(3-bromophenyl)-5,9-dimethyl-5,9-undecadiene

Guidance literature:: With thionyl chloride; In Petroleum ether; at -15 ℃; for 2h; under 520 - 560 Torr;
DOI:10.1021/jo972237s

Reference yield:

: 3132-99-8
m-bromobenzoic aldehyde

: 205117-90-4
1-chloro-1-(3-bromophenyl)-5,9-dimethyl-5,9-undecadiene

Guidance literature:: Multi-step reaction with 2 steps

1: 4 percent / lithium; CH₃I / tetrahydrofuran / 0 °C / sonication

2: thionyl chloride / petroleum ether / 2 h / -15 °C / 520 - 560 Torr

With thionyl chloride; lithium; methyl iodide; In tetrahydrofuran; Petroleum ether; 1: Barbier reaction / 2: Chlorination;
DOI:10.1021/jo972237s

Reference yield:

: 120060-00-6
10-bromo-3,7-dimethyl-2,6-decadiene

: 205117-90-4
1-chloro-1-(3-bromophenyl)-5,9-dimethyl-5,9-undecadiene

Guidance literature:: Multi-step reaction with 2 steps

1: 4 percent / lithium; CH₃I / tetrahydrofuran / 0 °C / sonication

2: thionyl chloride / petroleum ether / 2 h / -15 °C / 520 - 560 Torr

With thionyl chloride; lithium; methyl iodide; In tetrahydrofuran; Petroleum ether; 1: Barbier reaction / 2: Chlorination;
DOI:10.1021/jo972237s