C₂₉H₄₄N₂O₄Si

Base Information

Chemical Name:C₂₉H₄₄N₂O₄Si
CAS No.:1313867-88-7
Molecular Formula:C₂₉H₄₄N₂O₄Si
Molecular Weight:512.765
Hs Code.:

C<sub>29</sub>H<sub>44</sub>N<sub>2</sub>O<sub>4</sub>Si

Synonyms:C₂₉H₄₄N₂O₄Si

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Chemical Property of C₂₉H₄₄N₂O₄Si

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Technology Process of C₂₉H₄₄N₂O₄Si

There total 5 articles about C₂₉H₄₄N₂O₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 1313867-87-6
C₃₂H₅₂N₂O₄Si₂

: 1313867-89-8
C₂₆H₃₆N₂O₄

: 1313867-88-7
C₂₉H₄₄N₂O₄Si

Guidance literature:: With potassium carbonate; In methanol; dichloromethane; at 20 ℃; for 0.0833333h; Inert atmosphere;
DOI:10.1002/chem.201003603

Reference yield:

: 1313867-85-4
C₂₂H₃₆N₂O₄

: 1313867-88-7
C₂₉H₄₄N₂O₄Si

Guidance literature:: Multi-step reaction with 3 steps

1: iron(III) chloride; bromine / dichloromethane / Reflux

2: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / tetrahydrofuran / 70 °C / Inert atmosphere

3: potassium carbonate / methanol; dichloromethane / 0.08 h / 20 °C / Inert atmosphere

With iron(III) chloride; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; bromine; potassium carbonate; triethylamine; In tetrahydrofuran; methanol; dichloromethane; 2: Sonogashira coupling;
DOI:10.1002/chem.201003603

Reference yield:

: 1313867-86-5
C₂₂H₃₄Br₂N₂O₄

: 1313867-88-7
C₂₉H₄₄N₂O₄Si

Guidance literature:: Multi-step reaction with 2 steps

1: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / tetrahydrofuran / 70 °C / Inert atmosphere

2: potassium carbonate / methanol; dichloromethane / 0.08 h / 20 °C / Inert atmosphere

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; triethylamine; In tetrahydrofuran; methanol; dichloromethane; 1: Sonogashira coupling;
DOI:10.1002/chem.201003603