dimethyl-thiocarbamic acid S-[2-formyl-4-nitro-6-(1,4,7,10,13-pentaoxa-16-aza-cyclooctadec-16-ylmethyl)-phenyl] ester

Base Information

Chemical Name:dimethyl-thiocarbamic acid S-[2-formyl-4-nitro-6-(1,4,7,10,13-pentaoxa-16-aza-cyclooctadec-16-ylmethyl)-phenyl] ester
CAS No.:288852-77-7
Molecular Formula:C₂₃H₃₅N₃O₉S
Molecular Weight:529.612
Hs Code.:

dimethyl-thiocarbamic acid <i>S</i>-[2-formyl-4-nitro-6-(1,4,7,10,13-pentaoxa-16-aza-cyclooctadec-16-ylmethyl)-phenyl] ester

Synonyms:dimethyl-thiocarbamic acid S-[2-formyl-4-nitro-6-(1,4,7,10,13-pentaoxa-16-aza-cyclooctadec-16-ylmethyl)-phenyl] ester

Suppliers and Price of dimethyl-thiocarbamic acid S-[2-formyl-4-nitro-6-(1,4,7,10,13-pentaoxa-16-aza-cyclooctadec-16-ylmethyl)-phenyl] ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of dimethyl-thiocarbamic acid S-[2-formyl-4-nitro-6-(1,4,7,10,13-pentaoxa-16-aza-cyclooctadec-16-ylmethyl)-phenyl] ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of dimethyl-thiocarbamic acid S-[2-formyl-4-nitro-6-(1,4,7,10,13-pentaoxa-16-aza-cyclooctadec-16-ylmethyl)-phenyl] ester

There total 4 articles about dimethyl-thiocarbamic acid S-[2-formyl-4-nitro-6-(1,4,7,10,13-pentaoxa-16-aza-cyclooctadec-16-ylmethyl)-phenyl] ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 33941-15-0
1-aza-18-crown-6

: 288852-77-7
dimethyl-thiocarbamic acid S-[2-formyl-4-nitro-6-(1,4,7,10,13-pentaoxa-16-aza-cyclooctadec-16-ylmethyl)-phenyl] ester

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / tetrahydrofuran / 15 h / 0 - 20 °C

2: triethylamine / dimethylformamide / 15 h / 0 - 20 °C

3: toluene / 6 h / Heating

With triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide; toluene; 1: Alkylation / 2: Substitution / 3: Isomerization;
DOI:10.1021/jo000175r

Reference yield:

: 16644-30-7
3-(chloromethyl)-2-hydroxy-5-nitrobenzaldehyde

: 288852-77-7
dimethyl-thiocarbamic acid S-[2-formyl-4-nitro-6-(1,4,7,10,13-pentaoxa-16-aza-cyclooctadec-16-ylmethyl)-phenyl] ester

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / tetrahydrofuran / 15 h / 0 - 20 °C

2: triethylamine / dimethylformamide / 15 h / 0 - 20 °C

3: toluene / 6 h / Heating

With triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide; toluene; 1: Alkylation / 2: Substitution / 3: Isomerization;
DOI:10.1021/jo000175r

Reference yield:

: 141620-26-0
16-(3-formyl-2-hydroxy-5-nitrobenzyl)-1,4,7,10,13-pentaoxa-16-azacyclooctadecane

: 288852-77-7
dimethyl-thiocarbamic acid S-[2-formyl-4-nitro-6-(1,4,7,10,13-pentaoxa-16-aza-cyclooctadec-16-ylmethyl)-phenyl] ester

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dimethylformamide / 15 h / 0 - 20 °C

2: toluene / 6 h / Heating

With triethylamine; In N,N-dimethyl-formamide; toluene; 1: Substitution / 2: Isomerization;
DOI:10.1021/jo000175r