di-tert-butyl 1-(dimethylamino)-3-(2,5-dimethylphenyl)-3-oxoprop-1-en-2-yliminodicarbonate

Base Information

Chemical Name:di-tert-butyl 1-(dimethylamino)-3-(2,5-dimethylphenyl)-3-oxoprop-1-en-2-yliminodicarbonate
CAS No.:1224944-65-3
Molecular Formula:C₂₃H₃₄N₂O₅
Molecular Weight:418.533
Hs Code.:

Synonyms:di-tert-butyl 1-(dimethylamino)-3-(2,5-dimethylphenyl)-3-oxoprop-1-en-2-yliminodicarbonate

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Chemical Property of di-tert-butyl 1-(dimethylamino)-3-(2,5-dimethylphenyl)-3-oxoprop-1-en-2-yliminodicarbonate

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Technology Process of di-tert-butyl 1-(dimethylamino)-3-(2,5-dimethylphenyl)-3-oxoprop-1-en-2-yliminodicarbonate

There total 3 articles about di-tert-butyl 1-(dimethylamino)-3-(2,5-dimethylphenyl)-3-oxoprop-1-en-2-yliminodicarbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 1224944-64-2
di-tert-butyl 2-(2,5-dimethylphenyl)-2-oxoethyliminodicarbonate

: 1224944-65-3
di-tert-butyl 1-(dimethylamino)-3-(2,5-dimethylphenyl)-3-oxoprop-1-en-2-yliminodicarbonate

Guidance literature:: With N,N-dimethyl-formamide dimethyl acetal; at 70 - 100 ℃; for 41h;

Reference yield: 38.0%

: 1224944-64-2
di-tert-butyl 2-(2,5-dimethylphenyl)-2-oxoethyliminodicarbonate

: 4637-24-5
N,N-dimethyl-formamide dimethyl acetal

: 1224944-65-3
di-tert-butyl 1-(dimethylamino)-3-(2,5-dimethylphenyl)-3-oxoprop-1-en-2-yliminodicarbonate

Guidance literature:: at 70 - 100 ℃; for 41h; Inert atmosphere;

Reference yield:

: 51779-32-9
iminodicarboxylic acid di-tert-butyl ester

: 75840-13-0
2-bromo-1-(2,5-dimethylphenyl)ethan-1-one

: 1224944-65-3
di-tert-butyl 1-(dimethylamino)-3-(2,5-dimethylphenyl)-3-oxoprop-1-en-2-yliminodicarbonate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1.5 h / 20 °C

1.2: 1.5 h / 20 °C

2.1: N,N-dimethyl-formamide dimethyl acetal / 41 h / 70 - 100 °C

With sodium hydride; N,N-dimethyl-formamide dimethyl acetal; In N,N-dimethyl-formamide; mineral oil;