4-(2-furyl)butanoic acid pentafluorophenylic ester

Base Information

Chemical Name:4-(2-furyl)butanoic acid pentafluorophenylic ester
CAS No.:1577186-75-4
Molecular Formula:C₁₄H₉F₅O₃
Molecular Weight:320.216
Hs Code.:

Synonyms:4-(2-furyl)butanoic acid pentafluorophenylic ester

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Chemical Property of 4-(2-furyl)butanoic acid pentafluorophenylic ester

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Technology Process of 4-(2-furyl)butanoic acid pentafluorophenylic ester

There total 3 articles about 4-(2-furyl)butanoic acid pentafluorophenylic ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 92638-98-7
4-(furan-2-yl)butyric acid

: 771-61-9
2,3,4,5,6-pentafluorophenol

: 1577186-75-4
4-(2-furyl)butanoic acid pentafluorophenylic ester

Guidance literature:: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; at 0 - 20 ℃; for 18.5h; Inert atmosphere;
DOI:10.1021/ol500364j

Reference yield:

: 90005-38-2
4-(furan-2-yl)butanenitrile

: 1577186-75-4
4-(2-furyl)butanoic acid pentafluorophenylic ester

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydroxide; water / ethanol / 24 h / Reflux

2: triethylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / tetrahydrofuran / 18.5 h / 0 - 20 °C / Inert atmosphere

With water; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; potassium hydroxide; In tetrahydrofuran; ethanol;
DOI:10.1021/ol500364j

Reference yield:

: 92513-83-2
furnish 2-(3-bromopropyl)furan

: 1577186-75-4
4-(2-furyl)butanoic acid pentafluorophenylic ester

Guidance literature:: Multi-step reaction with 3 steps

1: dimethyl sulfoxide / 18 h / 70 °C / Inert atmosphere

2: potassium hydroxide; water / ethanol / 24 h / Reflux

3: triethylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / tetrahydrofuran / 18.5 h / 0 - 20 °C / Inert atmosphere

With water; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; potassium hydroxide; In tetrahydrofuran; ethanol; dimethyl sulfoxide;
DOI:10.1021/ol500364j