methyl (E)-4-{4-[2-(methyl-2-pyrimidylamino)ethoxy]benzyloxyimino}-4-phenylbutyrate

Base Information

Chemical Name:methyl (E)-4-{4-[2-(methyl-2-pyrimidylamino)ethoxy]benzyloxyimino}-4-phenylbutyrate
CAS No.:250601-47-9
Molecular Formula:C₂₅H₂₈N₄O₄
Molecular Weight:448.522
Hs Code.:

Synonyms:methyl (E)-4-{4-[2-(methyl-2-pyrimidylamino)ethoxy]benzyloxyimino}-4-phenylbutyrate

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Chemical Property of methyl (E)-4-{4-[2-(methyl-2-pyrimidylamino)ethoxy]benzyloxyimino}-4-phenylbutyrate

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Technology Process of methyl (E)-4-{4-[2-(methyl-2-pyrimidylamino)ethoxy]benzyloxyimino}-4-phenylbutyrate

There total 7 articles about methyl (E)-4-{4-[2-(methyl-2-pyrimidylamino)ethoxy]benzyloxyimino}-4-phenylbutyrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 250602-56-3
methyl (E)-4-hydroxyimino-4-phenylbutyrate

: 250602-80-3
4-[2-(methyl-2-pyrimidylamino)ethoxy]benzyl alcohol

: 250601-47-9
methyl (E)-4-{4-[2-(methyl-2-pyrimidylamino)ethoxy]benzyloxyimino}-4-phenylbutyrate

Guidance literature:: With hydrogenchloride; thionyl chloride; sodium chloride; sodium hydrogencarbonate; In N,N-dimethyl-formamide; toluene;

Reference yield:

: 250602-56-3
methyl (E)-4-hydroxyimino-4-phenylbutyrate

: [2-(4-chloromethyl-phenoxy)-ethyl]-methyl-pyrimidin-2-yl-amine

: 250601-47-9
methyl (E)-4-{4-[2-(methyl-2-pyrimidylamino)ethoxy]benzyloxyimino}-4-phenylbutyrate

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 2h;
DOI:10.1248/cpb.51.138

Reference yield:

: 122320-78-9
4-[2-(N-Methyl-N-(2-pyrimidinyl)amino)ethoxy]-benzaldehyde

: 250601-47-9
methyl (E)-4-{4-[2-(methyl-2-pyrimidylamino)ethoxy]benzyloxyimino}-4-phenylbutyrate

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / sodium borohydride / methanol; tetrahydrofuran / 0.5 h / 20 °C

2: thionyl chloride / toluene / 0.5 h / 20 °C

3: sodium hydride / dimethylformamide / 2 h / 0 °C

With sodium tetrahydroborate; thionyl chloride; sodium hydride; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; toluene;
DOI:10.1248/cpb.51.138