H₃CC(CH₂OC₆H₄NC)3

Base Information

Chemical Name:H₃CC(CH₂OC₆H₄NC)3
CAS No.:154120-63-5
Molecular Formula:C₂₆H₂₁N₃O₃
Molecular Weight:423.471
Hs Code.:

H<sub>3</sub>CC(CH<sub>2</sub>OC<sub>6</sub>H<sub>4</sub>NC)3

Synonyms:H₃CC(CH₂OC₆H₄NC)3

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Chemical Property of H₃CC(CH₂OC₆H₄NC)3

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Technology Process of H₃CC(CH₂OC₆H₄NC)3

There total 5 articles about H₃CC(CH₂OC₆H₄NC)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 154120-61-3
C₂₆H₂₇N₃O₆

: 154120-63-5
H₃CC(CH₂OC₆H₄NC)3

Guidance literature:: With triethylamine; trichloromethyl chloroformate; In dichloromethane; Ambient temperature;
DOI:10.1016/0022-328X(94)88014-X

Reference yield:

: 111770-00-4
2-methyl-2-{{(methylsulfonyl)oxy}methyl}-1,3-propanediol dimethanesulfonate

: 154120-63-5
H₃CC(CH₂OC₆H₄NC)3

Guidance literature:: Multi-step reaction with 4 steps

1: 54 percent / Kaliumcarbonat / dimethylformamide / 24 h / 135 °C

2: 93 percent / H₂ / 10percent Pd/C / tetrahydrofuran / 12 h / 75006 Torr

3: 72 percent / diethyl ether / 3 h

4: 90 percent / Triethylamin, Diphosgen / CH₂Cl₂ / Ambient temperature

With hydrogen; potassium carbonate; triethylamine; trichloromethyl chloroformate; palladium on activated charcoal; In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/0022-328X(94)88014-X

Reference yield:

: 154120-69-1
C₂₃H₂₁N₃O₉

: 154120-63-5
H₃CC(CH₂OC₆H₄NC)3

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / H₂ / 10percent Pd/C / tetrahydrofuran / 12 h / 75006 Torr

2: 72 percent / diethyl ether / 3 h

3: 90 percent / Triethylamin, Diphosgen / CH₂Cl₂ / Ambient temperature

With hydrogen; triethylamine; trichloromethyl chloroformate; palladium on activated charcoal; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1016/0022-328X(94)88014-X