C₃₃H₄₂N₈O₁₁

Base Information

Chemical Name:C₃₃H₄₂N₈O₁₁
CAS No.:1415917-87-1
Molecular Formula:C₃₃H₄₂N₈O₁₁
Molecular Weight:726.743
Hs Code.:

C<sub>33</sub>H<sub>42</sub>N<sub>8</sub>O<sub>11</sub>

Synonyms:C₃₃H₄₂N₈O₁₁

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Chemical Property of C₃₃H₄₂N₈O₁₁

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Technology Process of C₃₃H₄₂N₈O₁₁

There total 13 articles about C₃₃H₄₂N₈O₁₁ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: C₂₀H₂₄N₄O₇

: C₁₃H₂₀N₄O₅

: 1415917-87-1
C₃₃H₄₂N₈O₁₁

Guidance literature:: C₂₀H₂₄N₄O₇; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 0 ℃; for 1h;

C₁₃H₂₀N₄O₅; In dichloromethane; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1039/c2cc36566a

Reference yield:

: C₁₆H₂₄N₆O₅

: 1415917-87-1
C₃₃H₄₂N₈O₁₁

Guidance literature:: Multi-step reaction with 6 steps

1.1: triethylamine; tin(II) chloride hydrate; thiophenol / acetonitrile / 20 °C

2.1: sodium hydrogencarbonate / water; methanol / 2 h / 0 °C

3.1: water; acetic acid / 20 °C

4.1: sodium periodate / water; methanol / 5 h / 0 °C

5.1: sodium chlorite; sodium dihydrogenphosphate; dihydrogen peroxide / water; acetonitrile / 0 - 20 °C

6.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 1 h / 0 °C

6.2: 24 h / 20 °C / Inert atmosphere

With sodium chlorite; sodium periodate; sodium dihydrogenphosphate; tin(II) chloride hydrate; water; dihydrogen peroxide; sodium hydrogencarbonate; benzotriazol-1-ol; acetic acid; thiophenol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In methanol; dichloromethane; water; acetonitrile;
DOI:10.1039/c2cc36566a

Reference yield:

: C₁₆H₂₆N₄O₅

: 1415917-87-1
C₃₃H₄₂N₈O₁₁

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydrogencarbonate / water; methanol / 2 h / 0 °C

2.1: water; acetic acid / 20 °C

3.1: sodium periodate / water; methanol / 5 h / 0 °C

4.1: sodium chlorite; sodium dihydrogenphosphate; dihydrogen peroxide / water; acetonitrile / 0 - 20 °C

5.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 1 h / 0 °C

5.2: 24 h / 20 °C / Inert atmosphere

With sodium chlorite; sodium periodate; sodium dihydrogenphosphate; water; dihydrogen peroxide; sodium hydrogencarbonate; benzotriazol-1-ol; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In methanol; dichloromethane; water; acetonitrile;
DOI:10.1039/c2cc36566a