N-but-2-enyl-2,2,2-trifluoro-N-(2-iodo-4-trifluoromethyl-phenyl)-acetamide

Base Information

Chemical Name:N-but-2-enyl-2,2,2-trifluoro-N-(2-iodo-4-trifluoromethyl-phenyl)-acetamide
CAS No.:1068975-72-3
Molecular Formula:C₁₃H₁₀F₆INO
Molecular Weight:437.123
Hs Code.:

Synonyms:N-but-2-enyl-2,2,2-trifluoro-N-(2-iodo-4-trifluoromethyl-phenyl)-acetamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-but-2-enyl-2,2,2-trifluoro-N-(2-iodo-4-trifluoromethyl-phenyl)-acetamide

Chemical Property:

Purity/Quality:

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Technology Process of N-but-2-enyl-2,2,2-trifluoro-N-(2-iodo-4-trifluoromethyl-phenyl)-acetamide

There total 2 articles about N-but-2-enyl-2,2,2-trifluoro-N-(2-iodo-4-trifluoromethyl-phenyl)-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 878133-04-1
2,2,2-trifluoro-N-(2-iodo-4-(trifluoromethyl)phenyl)acetamide

: 4784-77-4,39616-19-8,29576-14-5
(E)-1-Bromo-2-butene

: 1068975-72-3
N-but-2-enyl-2,2,2-trifluoro-N-(2-iodo-4-trifluoromethyl-phenyl)-acetamide

Guidance literature:: With potassium carbonate; In acetonitrile; for 2h; Heating / reflux;

Reference yield:

: 163444-17-5
2-iodo-4-(trifluoromethyl)aniline

: 1068975-72-3
N-but-2-enyl-2,2,2-trifluoro-N-(2-iodo-4-trifluoromethyl-phenyl)-acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / dichloromethane / 1 h / 20 °C

2: potassium carbonate / acetonitrile / 2 h / Heating / reflux

With pyridine; potassium carbonate; In dichloromethane; acetonitrile;

Reference yield:

: 1068975-72-3
N-but-2-enyl-2,2,2-trifluoro-N-(2-iodo-4-trifluoromethyl-phenyl)-acetamide

: 1068971-10-7
2-(3-fluoro-phenyl)-4-methyl-pyrimidine-5-carboxylic acid (3-ethyl-5-trifluoromethyl-indol-1-yl)-amide

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrabutyl-ammonium chloride / palladium diacetate / N,N-dimethyl-formamide / 2 h / 100 °C

2.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 0 °C

2.2: 2 h / 0 - 20 °C

2.3: 0 °C

3.1: N,N-dimethyl-formamide / 1 h / 50 °C

3.2: 2 h / 50 °C

With tetrabutyl-ammonium chloride; sodium hydride; palladium diacetate; In N,N-dimethyl-formamide;