(4-((methoxymethoxy)methyl)-3-bromophenyl)(3,4-dichlorophenyl)sulfide

Base Information

Chemical Name:(4-((methoxymethoxy)methyl)-3-bromophenyl)(3,4-dichlorophenyl)sulfide
CAS No.:1222010-78-7
Molecular Formula:C₁₅H₁₃BrCl₂O₂S
Molecular Weight:408.143
Hs Code.:

Synonyms:(4-((methoxymethoxy)methyl)-3-bromophenyl)(3,4-dichlorophenyl)sulfide

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Chemical Property of (4-((methoxymethoxy)methyl)-3-bromophenyl)(3,4-dichlorophenyl)sulfide

Chemical Property:

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Technology Process of (4-((methoxymethoxy)methyl)-3-bromophenyl)(3,4-dichlorophenyl)sulfide

There total 5 articles about (4-((methoxymethoxy)methyl)-3-bromophenyl)(3,4-dichlorophenyl)sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1222010-77-6
4-((3,4-dichlorophenyl)thio)-2-bromobenzyl alcohol

: 107-30-2
chloromethyl methyl ether

: 1222010-78-7
(4-((methoxymethoxy)methyl)-3-bromophenyl)(3,4-dichlorophenyl)sulfide

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; for 14h; Inert atmosphere;

Reference yield:

: 59142-68-6
2-bromo-4-fluorobenzaldehyde

: 1222010-78-7
(4-((methoxymethoxy)methyl)-3-bromophenyl)(3,4-dichlorophenyl)sulfide

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / N,N-dimethyl-formamide / 0.5 h / 0 °C / Inert atmosphere

2: methanol; sodium tetrahydroborate / 0.5 h / 0 °C / Inert atmosphere

3: N-ethyl-N,N-diisopropylamine / dichloromethane / 14 h / Inert atmosphere

With methanol; sodium tetrahydroborate; potassium carbonate; N-ethyl-N,N-diisopropylamine; In dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 1222010-76-5
4-((3,4-dichlorophenyl)thio)-2-bromobenzaldehyde

: 1222010-78-7
(4-((methoxymethoxy)methyl)-3-bromophenyl)(3,4-dichlorophenyl)sulfide

Guidance literature:: Multi-step reaction with 2 steps

1: methanol; sodium tetrahydroborate / 0.5 h / 0 °C / Inert atmosphere

2: N-ethyl-N,N-diisopropylamine / dichloromethane / 14 h / Inert atmosphere

With methanol; sodium tetrahydroborate; N-ethyl-N,N-diisopropylamine; In dichloromethane;