O-triethylsilyl-2-(4-benzyloxy-3-methoxyphenyl)-4,5-methylenedioxybenzyl alcohol

Base Information

Chemical Name:O-triethylsilyl-2-(4-benzyloxy-3-methoxyphenyl)-4,5-methylenedioxybenzyl alcohol
CAS No.:438036-63-6
Molecular Formula:C₂₈H₃₄O₅Si
Molecular Weight:478.66
Hs Code.:

Synonyms:O-triethylsilyl-2-(4-benzyloxy-3-methoxyphenyl)-4,5-methylenedioxybenzyl alcohol

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Chemical Property of O-triethylsilyl-2-(4-benzyloxy-3-methoxyphenyl)-4,5-methylenedioxybenzyl alcohol

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Technology Process of O-triethylsilyl-2-(4-benzyloxy-3-methoxyphenyl)-4,5-methylenedioxybenzyl alcohol

There total 3 articles about O-triethylsilyl-2-(4-benzyloxy-3-methoxyphenyl)-4,5-methylenedioxybenzyl alcohol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 21.0%

: 438036-61-4
5-(triethylsilyloxymethyl)-6-iodo-1,3-benzodioxole

: 3-methoxy-4-benzyloxy-1-tributylstannylbenzene

: 438036-63-6
O-triethylsilyl-2-(4-benzyloxy-3-methoxyphenyl)-4,5-methylenedioxybenzyl alcohol

Guidance literature:: With 10percent Pd(PPh₃)4; In toluene; for 96h; Heating;
DOI:10.1021/jo020010d

Reference yield:

: 69048-76-6
6-iodo-1,3-benzodioxole-5-methanol

: 438036-63-6
O-triethylsilyl-2-(4-benzyloxy-3-methoxyphenyl)-4,5-methylenedioxybenzyl alcohol

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / Et₃N / CH₂Cl₂ / 4 h / 0 - 20 °C

2: 21 percent / 10percent Pd(PPh₃)4 / toluene / 96 h / Heating

With triethylamine; In dichloromethane; toluene;
DOI:10.1021/jo020010d

Reference yield:

: 79271-56-0
triethylsilyl trifluoromethyl sulfonate

: 438036-63-6
O-triethylsilyl-2-(4-benzyloxy-3-methoxyphenyl)-4,5-methylenedioxybenzyl alcohol

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / Et₃N / CH₂Cl₂ / 4 h / 0 - 20 °C

2: 21 percent / 10percent Pd(PPh₃)4 / toluene / 96 h / Heating

With triethylamine; In dichloromethane; toluene;
DOI:10.1021/jo020010d