Technology Process of N,N'-bistosyl-5,13-diaza-1,9-dithiacyclohexadecane
There total 3 articles about N,N'-bistosyl-5,13-diaza-1,9-dithiacyclohexadecane which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
caesium carbonate;
In
N,N-dimethyl-formamide;
at 30 ℃;
for 30h;
Inert atmosphere;
DOI:10.1080/10610278.2011.575468
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium iodide / acetone / 3 h / Inert atmosphere; Reflux
2: caesium carbonate / N,N-dimethyl-formamide / 30 h / 30 °C / Inert atmosphere
With
caesium carbonate; sodium iodide;
In
N,N-dimethyl-formamide; acetone;
DOI:10.1080/10610278.2011.575468
- Guidance literature:
-
Multi-step reaction with 3 steps
1: dichloromethane; acetonitrile / 72 h / 40 °C / Inert atmosphere
2: hydrogenchloride; water / ethanol / 24 h / Inert atmosphere; Reflux
3: caesium carbonate / N,N-dimethyl-formamide / 30 h / 30 °C / Inert atmosphere
With
hydrogenchloride; water; caesium carbonate;
In
ethanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1080/10610278.2011.575468
