3-bromo-2-iodo-9,9-diimethyl-9H-fluorene

Base Information

Chemical Name:3-bromo-2-iodo-9,9-diimethyl-9H-fluorene
CAS No.:1346635-65-1
Molecular Formula:C₁₅H₁₂BrI
Molecular Weight:399.069
Hs Code.:

Synonyms:3-bromo-2-iodo-9,9-diimethyl-9H-fluorene

Suppliers and Price of 3-bromo-2-iodo-9,9-diimethyl-9H-fluorene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 4 raw suppliers

Chemical Property of 3-bromo-2-iodo-9,9-diimethyl-9H-fluorene

Chemical Property:

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

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Technology Process of 3-bromo-2-iodo-9,9-diimethyl-9H-fluorene

There total 2 articles about 3-bromo-2-iodo-9,9-diimethyl-9H-fluorene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 3-bromo-9,9-dimethyl-9H-fluorene-2-amine

: 1346635-65-1
3-bromo-2-iodo-9,9-diimethyl-9H-fluorene

Guidance literature:: 3-bromo-9,9-dimethyl-9H-fluorene-2-amine; With sulfuric acid; at 20 ℃; for 1h;

With potassium iodide; sodium nitrite; at 0 - 20 ℃; for 1h;

Reference yield:

: 108714-73-4
9,9-dimethyl-9H-fluoren-2-ylamine

: 1346635-65-1
3-bromo-2-iodo-9,9-diimethyl-9H-fluorene

Guidance literature:: Multi-step reaction with 2 steps

1.1: N-Bromosuccinimide / N,N-dimethyl-formamide / 0 - 20 °C

2.1: sulfuric acid / 1 h / 20 °C

2.2: 1 h / 0 - 20 °C

With N-Bromosuccinimide; sulfuric acid; In N,N-dimethyl-formamide;

Reference yield: 77.6%

: 1346635-65-1
3-bromo-2-iodo-9,9-diimethyl-9H-fluorene

: 349666-24-6
1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyrene

: 1346635-67-3
C₃₁H₂₁Br

Guidance literature:: With water; caesium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In ethanol; toluene; at 77 ℃; for 5h; Inert atmosphere;