Technology Process of C17H20FNO3
There total 8 articles about C17H20FNO3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
ammonium formate; palladium(II) hydroxide;
In
ethanol;
at 65 ℃;
for 0.333333h;
Inert atmosphere;
DOI:10.1021/jm301113w
- Guidance literature:
-
Multi-step reaction with 7 steps
1: boron tribromide / dichloromethane / 6 h / -78 - -20 °C / Inert atmosphere
2: potassium carbonate; sodium iodide / acetone / 5 h / 40 °C / Inert atmosphere
3: magnesium / methanol / 20 °C / Inert atmosphere
4: potassium hydroxide / acetonitrile / 2 h / 80 °C
5: tin(ll) chloride; hydrogenchloride / diethyl ether / 0 - 20 °C / Inert atmosphere
6: potassium carbonate / N,N-dimethyl-formamide / 2 h / 180 °C / Microwave irradiation
7: palladium(II) hydroxide; ammonium formate / ethanol / 0.33 h / 65 °C / Inert atmosphere
With
hydrogenchloride; ammonium formate; palladium(II) hydroxide; boron tribromide; potassium carbonate; magnesium; sodium iodide; tin(ll) chloride; potassium hydroxide;
In
methanol; diethyl ether; ethanol; dichloromethane; N,N-dimethyl-formamide; acetone; acetonitrile;
DOI:10.1021/jm301113w
- Guidance literature:
-
Multi-step reaction with 6 steps
1: potassium carbonate; sodium iodide / acetone / 5 h / 40 °C / Inert atmosphere
2: magnesium / methanol / 20 °C / Inert atmosphere
3: potassium hydroxide / acetonitrile / 2 h / 80 °C
4: tin(ll) chloride; hydrogenchloride / diethyl ether / 0 - 20 °C / Inert atmosphere
5: potassium carbonate / N,N-dimethyl-formamide / 2 h / 180 °C / Microwave irradiation
6: palladium(II) hydroxide; ammonium formate / ethanol / 0.33 h / 65 °C / Inert atmosphere
With
hydrogenchloride; ammonium formate; palladium(II) hydroxide; potassium carbonate; magnesium; sodium iodide; tin(ll) chloride; potassium hydroxide;
In
methanol; diethyl ether; ethanol; N,N-dimethyl-formamide; acetone; acetonitrile;
DOI:10.1021/jm301113w