Benzo[1,3]dioxol-5-yl-((3S,4R,5S)-5-benzo[1,3]dioxol-5-yl-4-benzyloxymethyl-tetrahydro-furan-3-yl)-methanol

Base Information

• Chemical Name: Benzo[1,3]dioxol-5-yl-((3S,4R,5S)-5-benzo[1,3]dioxol-5-yl-4-benzyloxymethyl-tetrahydro-furan-3-yl)-methanol
• CAS No.: 337968-49-7
• Molecular Formula: C₂₇H₂₆O₇
• Molecular Weight: 462.499

Synonyms:Benzo[1,3]dioxol-5-yl-((3S,4R,5S)-5-benzo[1,3]dioxol-5-yl-4-benzyloxymethyl-tetrahydro-furan-3-yl)-methanol

Chemical Property of Benzo[1,3]dioxol-5-yl-((3S,4R,5S)-5-benzo[1,3]dioxol-5-yl-4-benzyloxymethyl-tetrahydro-furan-3-yl)-methanol

Chemical Property:

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Technology Process of Benzo[1,3]dioxol-5-yl-((3S,4R,5S)-5-benzo[1,3]dioxol-5-yl-4-benzyloxymethyl-tetrahydro-furan-3-yl)-methanol

There total 1 articles about Benzo[1,3]dioxol-5-yl-((3S,4R,5S)-5-benzo[1,3]dioxol-5-yl-4-benzyloxymethyl-tetrahydro-furan-3-yl)-methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

Acetic acid benzo[1,3]dioxol-5-yl-((3S,4R,5S)-5-benzo[1,3]dioxol-5-yl-4-benzyloxymethyl-tetrahydro-furan-3-yl)-methyl ester (337968-35-1) → Benzo[1,3]dioxol-5-yl-((3S,4R,5S)-5-benzo[1,3]dioxol-5-yl-4-benzyloxymethyl-tetrahydro-furan-3-yl)-methanol (337968-49-7)

Guidance literature:

With methanol; potassium carbonate;

DOI:10.1055/s-2001-11419

Reference yield: 72.0%

Benzo[1,3]dioxol-5-yl-((3S,4R,5S)-5-benzo[1,3]dioxol-5-yl-4-benzyloxymethyl-tetrahydro-furan-3-yl)-methanol (337968-49-7) → Benzo[1,3]dioxol-5-yl-((3S,4R,5S)-5-benzo[1,3]dioxol-5-yl-4-benzyloxymethyl-tetrahydro-furan-3-yl)-methanone

Guidance literature:

With N-methyl-2-indolinone; tetrapropylammonium perruthennate; In dichloromethane;

DOI:10.1055/s-2001-11419

Reference yield:

Benzo[1,3]dioxol-5-yl-((3S,4R,5S)-5-benzo[1,3]dioxol-5-yl-4-benzyloxymethyl-tetrahydro-furan-3-yl)-methanol (337968-49-7) → sesaminone (157207-93-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 72 percent / TPAP; NMO / CH₂Cl₂

2: 82 percent / HCOOH / Pd black

With formic acid; N-methyl-2-indolinone; tetrapropylammonium perruthennate; palladium; In dichloromethane;

DOI:10.1055/s-2001-11419

upstream raw materials:

Acetic acid benzo[1,3]dioxol-5-yl-((3S,4R,5S)-5-benzo[1,3]dioxol-5-yl-4-benzyloxymethyl-tetrahydro-furan-3-yl)-methyl ester

Downstream raw materials:

sesaminone

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