Technology Process of C35H40O2S2
There total 7 articles about C35H40O2S2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C25H21IOS2;
With
n-butyllithium;
In
hexane; toluene;
at -30 ℃;
3,3,5,5-tetramethylcyclohexanone;
In
hexane; toluene;
at 0 ℃;
for 3h;
With
water;
In
hexane; toluene;
- Guidance literature:
-
Multi-step reaction with 9 steps
1.1: aluminum (III) chloride / dichloromethane / 0 °C
2.1: potassium tert-butylate / tetrahydrofuran / 55 °C
3.1: toluene / 3 h / Reflux
4.1: sodium hydroxide; water / methanol / 3 h / Reflux
5.1: potassium carbonate / N,N-dimethyl-formamide / 3 h / 60 °C
6.1: sodium hydroxide; water / isopropyl alcohol / 3 h / Reflux
7.1: triethylamine; diphenyl phosphoryl azide / toluene / 2 h / 20 °C
7.2: 2 h / 70 °C
7.3: 6 h / Reflux
8.1: hydrogenchloride; sodium nitrite / acetonitrile; water / 0 - 5 °C
8.2: 5 h / 20 °C
9.1: n-butyllithium / toluene; hexane / -30 °C
9.2: 3 h / 0 °C
With
hydrogenchloride; aluminum (III) chloride; n-butyllithium; diphenyl phosphoryl azide; potassium tert-butylate; water; potassium carbonate; triethylamine; sodium hydroxide; sodium nitrite;
In
tetrahydrofuran; methanol; hexane; dichloromethane; water; N,N-dimethyl-formamide; isopropyl alcohol; toluene; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: potassium tert-butylate / tetrahydrofuran / 55 °C
2.1: toluene / 3 h / Reflux
3.1: sodium hydroxide; water / methanol / 3 h / Reflux
4.1: potassium carbonate / N,N-dimethyl-formamide / 3 h / 60 °C
5.1: sodium hydroxide; water / isopropyl alcohol / 3 h / Reflux
6.1: triethylamine; diphenyl phosphoryl azide / toluene / 2 h / 20 °C
6.2: 2 h / 70 °C
6.3: 6 h / Reflux
7.1: hydrogenchloride; sodium nitrite / acetonitrile; water / 0 - 5 °C
7.2: 5 h / 20 °C
8.1: n-butyllithium / toluene; hexane / -30 °C
8.2: 3 h / 0 °C
With
hydrogenchloride; n-butyllithium; diphenyl phosphoryl azide; potassium tert-butylate; water; potassium carbonate; triethylamine; sodium hydroxide; sodium nitrite;
In
tetrahydrofuran; methanol; hexane; water; N,N-dimethyl-formamide; isopropyl alcohol; toluene; acetonitrile;