N-benzyl-N',N''-ethylene-N-[(methoxycarbonyl)methyl]-N',N''-dimethylguanidinium hexafluorophosphate

Base Information

Chemical Name:N-benzyl-N',N''-ethylene-N-[(methoxycarbonyl)methyl]-N',N''-dimethylguanidinium hexafluorophosphate
CAS No.:1452849-45-4
Molecular Formula:C₁₅H₂₂N₃O₂*F₆P
Molecular Weight:421.323
Hs Code.:

Synonyms:N-benzyl-N',N''-ethylene-N-[(methoxycarbonyl)methyl]-N',N''-dimethylguanidinium hexafluorophosphate

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Chemical Property of N-benzyl-N',N''-ethylene-N-[(methoxycarbonyl)methyl]-N',N''-dimethylguanidinium hexafluorophosphate

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Technology Process of N-benzyl-N',N''-ethylene-N-[(methoxycarbonyl)methyl]-N',N''-dimethylguanidinium hexafluorophosphate

There total 2 articles about N-benzyl-N',N''-ethylene-N-[(methoxycarbonyl)methyl]-N',N''-dimethylguanidinium hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₅H₂₂N₃O₂⁽¹⁺⁾*Br^(1-)

: 1452849-45-4
N-benzyl-N',N''-ethylene-N-[(methoxycarbonyl)methyl]-N',N''-dimethylguanidinium hexafluorophosphate

Guidance literature:: With ammonium hexafluorophosphate; In water;
DOI:10.1002/hlca.201200510

Reference yield:

: 25653-11-6
2-(benzylimino)-1,3-dimethylimidazolidine

: 1452849-45-4
N-benzyl-N',N''-ethylene-N-[(methoxycarbonyl)methyl]-N',N''-dimethylguanidinium hexafluorophosphate

Guidance literature:: Multi-step reaction with 2 steps

1: acetonitrile / 3 h / 20 °C

2: ammonium hexafluorophosphate / water

With ammonium hexafluorophosphate; In water; acetonitrile;
DOI:10.1002/hlca.201200510

Reference yield: 74.0%

: 1452849-46-5
3-({[(tert-butyl)(diphenyl)silyl]oxy}methyl)-1-(phenylsulfonyl)-1H-indole-2-carboxaldehyde

: 1452849-45-4
N-benzyl-N',N''-ethylene-N-[(methoxycarbonyl)methyl]-N',N''-dimethylguanidinium hexafluorophosphate

: methyl rac-(2R,3R)-3-[3-({[(tert-butyl)(diphenyl)silyl]oxy}methyl)-1-(phenylsulfonyl)-1H-indol-2-yl]-1-(phenylmethyl)aziridine-2-carboxylate

Guidance literature:: N-benzyl-N',N''-ethylene-N-[(methoxycarbonyl)methyl]-N',N''-dimethylguanidinium hexafluorophosphate; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at -20 ℃; for 0.5h; Inert atmosphere;

3-({[(tert-butyl)(diphenyl)silyl]oxy}methyl)-1-(phenylsulfonyl)-1H-indole-2-carboxaldehyde; In N,N-dimethyl-formamide; mineral oil; at -20 ℃; for 3.5h; Inert atmosphere;

With silica gel; In N,N-dimethyl-formamide; acetonitrile; mineral oil; at 20 ℃; for 22h; Inert atmosphere;
DOI:10.1002/hlca.201200510