N-(benzyloxycarbonyl)-3-<<(4-nitrobenzyl)oxy>-NNO-azoxy>-L-alanine 4-nitrobenzyl ester

Base Information

Chemical Name:N-(benzyloxycarbonyl)-3-<<(4-nitrobenzyl)oxy>-NNO-azoxy>-L-alanine 4-nitrobenzyl ester
CAS No.:90991-38-1
Molecular Formula:C₂₅H₂₃N₅O₁₀
Molecular Weight:553.485
Hs Code.:

Synonyms:N-(benzyloxycarbonyl)-3-<<(4-nitrobenzyl)oxy>-NNO-azoxy>-L-alanine 4-nitrobenzyl ester

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Chemical Property of N-(benzyloxycarbonyl)-3-<<(4-nitrobenzyl)oxy>-NNO-azoxy>-L-alanine 4-nitrobenzyl ester

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Technology Process of N-(benzyloxycarbonyl)-3-<<(4-nitrobenzyl)oxy>-NNO-azoxy>-L-alanine 4-nitrobenzyl ester

There total 2 articles about N-(benzyloxycarbonyl)-3-<<(4-nitrobenzyl)oxy>-NNO-azoxy>-L-alanine 4-nitrobenzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.5%

: 90991-36-9
N-(benzyloxycarbonyl)-3-(hydroxynitrosoamino)-L-alanine

: 100-11-8
1-bromomethyl-4-nitro-benzene

: 90991-38-1
N-(benzyloxycarbonyl)-3-<<(4-nitrobenzyl)oxy>-NNO-azoxy>-L-alanine 4-nitrobenzyl ester

Guidance literature:: With TEA; sodium sulfate; In ethyl acetate; for 96h; Ambient temperature;
DOI:10.1021/jm00376a012

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 90991-38-1
N-(benzyloxycarbonyl)-3-<<(4-nitrobenzyl)oxy>-NNO-azoxy>-L-alanine 4-nitrobenzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 47.6 percent / aq. NaOH / 6 h / 0 - 3 °C

2: 51.5 percent / TEA, Na₂SO₄ / ethyl acetate / 96 h / Ambient temperature

With sodium hydroxide; TEA; sodium sulfate; In ethyl acetate;
DOI:10.1021/jm00376a012