Technology Process of C23H28O5
There total 6 articles about C23H28O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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Multi-step reaction with 2 steps
1: dimethyl sulfoxide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dichloromethane / 3 h / 0 - 20 °C
2: dichloromethane / 2 h / 20 °C
With
dimethyl sulfoxide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione;
In
dichloromethane;
1: Swern oxidation;
DOI:10.1055/s-0030-1260546
- Guidance literature:
-
Multi-step reaction with 3 steps
1: toluene-4-sulfonic acid / methanol / 20 °C
2: dimethyl sulfoxide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dichloromethane / 3 h / 0 - 20 °C
3: dichloromethane / 2 h / 20 °C
With
toluene-4-sulfonic acid; dimethyl sulfoxide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione;
In
methanol; dichloromethane;
2: Swern oxidation;
DOI:10.1055/s-0030-1260546
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78469-85-9,78513-07-2,78513-15-2,84621-89-6,87172-27-8,95672-91-6,98048-62-5,98048-63-6,78513-12-9
(2S,3S)-4-benzyloxy-2,3-epoxy-1-butanol
- Guidance literature:
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Multi-step reaction with 5 steps
1.1: sodium bis(2-methoxyethoxy)aluminium dihydride / tetrahydrofuran / 12 h / 0 - 20 °C
2.1: 1H-imidazole / 12 h / 20 °C
2.2: 3.5 h / 0 - 20 °C
3.1: toluene-4-sulfonic acid / methanol / 20 °C
4.1: dimethyl sulfoxide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dichloromethane / 3 h / 0 - 20 °C
5.1: dichloromethane / 2 h / 20 °C
With
toluene-4-sulfonic acid; dimethyl sulfoxide; sodium bis(2-methoxyethoxy)aluminium dihydride; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione;
In
tetrahydrofuran; 1H-imidazole; methanol; dichloromethane;
4.1: Swern oxidation;
DOI:10.1055/s-0030-1260546