Technology Process of C20H23IN6O4
There total 10 articles about C20H23IN6O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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Multi-step reaction with 6 steps
1.1: triethylamine / ethanol / 20 °C
2.1: sodium methylate / methanol / 1 h / 20 °C
3.1: toluene-4-sulfonic acid / acetone / 0 - 20 °C
3.2: 0.5 h / 20 °C
4.1: dipyridinium dichromate / N,N-dimethyl-formamide / 20 h / 20 °C
5.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 12 h / 20 °C
6.1: hydrogenchloride; water / tetrahydrofuran / 12 h / 20 °C
With
hydrogenchloride; dipyridinium dichromate; water; sodium methylate; benzotriazol-1-ol; toluene-4-sulfonic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide; acetone;
DOI:10.5012/bkcs.2011.32.5.1620
- Guidance literature:
-
Multi-step reaction with 9 steps
1.1: dicobalt octacarbonyl / 0.17 h / 20 °C / 760.05 Torr
1.2: 15 h / 30 °C / 760.05 Torr
2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 0 - 20 °C
3.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere
3.2: 12 h / 20 °C
4.1: triethylamine / ethanol / 20 °C
5.1: sodium methylate / methanol / 1 h / 20 °C
6.1: toluene-4-sulfonic acid / acetone / 0 - 20 °C
6.2: 0.5 h / 20 °C
7.1: dipyridinium dichromate / N,N-dimethyl-formamide / 20 h / 20 °C
8.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 12 h / 20 °C
9.1: hydrogenchloride; water / tetrahydrofuran / 12 h / 20 °C
With
hydrogenchloride; dipyridinium dichromate; dicobalt octacarbonyl; di-isopropyl azodicarboxylate; tetrabutyl ammonium fluoride; water; sodium methylate; benzotriazol-1-ol; toluene-4-sulfonic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine;
In
tetrahydrofuran; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide; acetone;
3.1: Mitsunobu reaction / 3.2: Mitsunobu reaction;
DOI:10.5012/bkcs.2011.32.5.1620