4-HEXYLOXYBENZYLAMINE

Base Information

• Chemical Name: 4-HEXYLOXYBENZYLAMINE
• CAS No.: 4950-91-8
• Molecular Formula: C13H21 N O
• Molecular Weight: 207.316
• Mol file: 4950-91-8.mol

Synonyms:Benzylamine,p-(hexyloxy)- (7CI,8CI); 4-Hexyloxybenzylamine

Chemical Property of 4-HEXYLOXYBENZYLAMINE

Chemical Property:

• PSA: 35.25000
• LogP: 3.80470

Purity/Quality:

98%Min ^*data from raw suppliers

4-Hexyloxybenzylamine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-HEXYLOXYBENZYLAMINE

There total 4 articles about 4-HEXYLOXYBENZYLAMINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

1-(4-cyanophenyl)oxyhexane (66052-06-0) → [4-(hexyloxy)phenyl]methanamine (4950-91-8)

Guidance literature:

With hydrogen; pyrographite; palladium; In ethanol; at 20 ℃; for 2h;

DOI:10.1016/j.ejps.2004.03.003

Reference yield:

1-bromo-hexane (111-25-1) → [4-(hexyloxy)phenyl]methanamine (4950-91-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 56 percent / NaH / dimethylformamide / 45 h / 20 °C

2: 67 percent / H₂ / Pd; C / ethanol / 2 h / 20 °C

With hydrogen; sodium hydride; pyrographite; palladium; In ethanol; N,N-dimethyl-formamide;

DOI:10.1016/j.ejps.2004.03.003

Reference yield:

4-cyanophenol (767-00-0) → [4-(hexyloxy)phenyl]methanamine (4950-91-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 56 percent / NaH / dimethylformamide / 45 h / 20 °C

2: 67 percent / H₂ / Pd; C / ethanol / 2 h / 20 °C

With hydrogen; sodium hydride; pyrographite; palladium; In ethanol; N,N-dimethyl-formamide;

DOI:10.1016/j.ejps.2004.03.003

upstream raw materials:

1-(4-cyanophenyl)oxyhexane

1-bromo-hexane

4-cyanophenol

Downstream raw materials:

[Ag(NH₂CH₂C₆H₄OC₆H₁₃)2]⁽¹⁺⁾*BF₄^(1-)=[Ag(NH₂CH₂C₆H₄OC₆H₁₃)2][BF₄]

[Ag(NH₂CH₂C₆H₄OC₆H₁₃)2]⁽¹⁺⁾*NO₃^(1-)=[Ag(NH₂CH₂C₆H₄OC₆H₁₃)2][NO₃]

3-(4-hexyloxy-benzylcarbamoyl)-piperidine-1-carboxylic acid tert-butyl ester

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