4-[3-(4-chlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-5-yl]-2-methylaniline

Base Information

Chemical Name:4-[3-(4-chlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-5-yl]-2-methylaniline
CAS No.:666745-26-2
Molecular Formula:C₁₇H₁₄ClF₃N₂O
Molecular Weight:354.759
Hs Code.:

Synonyms:4-[3-(4-chlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-5-yl]-2-methylaniline

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Chemical Property of 4-[3-(4-chlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-5-yl]-2-methylaniline

Chemical Property:

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Technology Process of 4-[3-(4-chlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-5-yl]-2-methylaniline

There total 1 articles about 4-[3-(4-chlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-5-yl]-2-methylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 666746-31-2
t-butyl 4-[3-(4-chlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-5-yl]-2-methylcarbanilate

: 666745-26-2
4-[3-(4-chlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-5-yl]-2-methylaniline

Guidance literature:: t-butyl 4-[3-(4-chlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-5-yl]-2-methylcarbanilate; With trifluoroacetic acid; at 0 ℃; for 0.166667h;

With sodium hydrogencarbonate; In diethyl ether; water;

Reference yield:

: 666745-26-2
4-[3-(4-chlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-5-yl]-2-methylaniline

: 317813-24-4
3-iodo-N,N-diethylphthalamidic acid

: N₂,N₂-diethyl-3-iodo-N₁-[4-[3-(4-methylsulfonylphenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-5-yl]-2-methylphenyl]phthalic diamide

Guidance literature:: 3-iodo-N,N-diethylphthalamidic acid; With thionyl chloride; In chloroform; for 4h; Heating / reflux;

4-[3-(4-chlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-5-yl]-2-methylaniline; In acetonitrile; at 20 ℃; for 5h;

Reference yield:

: 666745-26-2
4-[3-(4-chlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-5-yl]-2-methylaniline

: 317813-26-6
3-iodo-N-(1-methyl-2-methylsulfanyl-ethyl)-phthalamic acid

: N₁-[4-[3-(4-chlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-5-yl]-2-methylphenyl]-3-iodo-N₂-(1-methyl-2-methylthioethyl)phthalic diamide

Guidance literature:: 3-iodo-N-(1-methyl-2-methylsulfanyl-ethyl)-phthalamic acid; With trifluoroacetic anhydride; In dichloromethane; at 0 ℃; for 2h;

4-[3-(4-chlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-5-yl]-2-methylaniline; In dichloromethane; at 20 ℃; for 12h;