C₁₉H₂₂O₆

Base Information

Chemical Name:C₁₉H₂₂O₆
CAS No.:1332271-54-1
Molecular Formula:C₁₉H₂₂O₆
Molecular Weight:346.38
Hs Code.:

C<sub>19</sub>H<sub>22</sub>O<sub>6</sub>

Synonyms:C₁₉H₂₂O₆

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Chemical Property of C₁₉H₂₂O₆

Chemical Property:

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Technology Process of C₁₉H₂₂O₆

There total 12 articles about C₁₉H₂₂O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₉H₂₂O₅

: 1332271-54-1
C₁₉H₂₂O₆

Guidance literature:: C₁₉H₂₂O₅; With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; In water; tert-butyl alcohol; at 20 ℃; for 2h; Inert atmosphere;

With triethylamine; In dichloromethane; for 3h; Inert atmosphere; Cooling with ice;
DOI:10.1016/j.tet.2011.04.094

Reference yield:

: 1308721-86-9
2-hydroxy-3-methyl-4,5-dimethoxybenzaldehyde

: 1332271-54-1
C₁₉H₂₂O₆

Guidance literature:: Multi-step reaction with 8 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 0 °C / Inert atmosphere

2.1: potassium tert-butylate / tetrahydrofuran / 2.08 h / -78 - 0 °C / Inert atmosphere

2.2: 16.08 h / 20 °C / Inert atmosphere

3.1: AD-mix-β; water / tert-butyl alcohol / 3 h / 20 °C / Inert atmosphere

4.1: dmap; triethylamine / dichloromethane / 18 h / 20 °C / Inert atmosphere

5.1: sodium hydride / tetrahydrofuran / 0.67 h / 0 - 20 °C / Inert atmosphere; Cooling with ice

5.2: 3 h / 20 °C / Inert atmosphere

6.1: triethylsilane; trifluoroacetic acid / dichloromethane / 0.17 h / 20 °C / Inert atmosphere

7.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.27 h / -78 °C / Inert atmosphere

7.2: 3.02 h / Inert atmosphere; Cooling with ice

8.1: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / water; tert-butyl alcohol / 2 h / 20 °C / Inert atmosphere

8.2: 3 h / Inert atmosphere; Cooling with ice

With triethylsilane; dmap; sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; oxalyl dichloride; AD-mix-β; potassium tert-butylate; water; sodium hydride; potassium carbonate; dimethyl sulfoxide; triethylamine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol; 3.1: Sharpless dihydroxylation / 7.1: Swern oxidation / 7.2: Swern oxidation / 8.1: Lindgren-Kraus oxidation;
DOI:10.1016/j.tet.2011.04.094

Reference yield:

: 1376220-15-3
(3,4-dimethoxy-2-methylphenoxy)methyl methyl ether

: 1332271-54-1
C₁₉H₂₂O₆

Guidance literature:: Multi-step reaction with 10 steps

1.1: hydrogenchloride / ethanol; water / Inert atmosphere

2.1: triethylamine; magnesium chloride / acetonitrile / 0.5 h / Inert atmosphere; Reflux

3.1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 0 °C / Inert atmosphere

4.1: potassium tert-butylate / tetrahydrofuran / 2.08 h / -78 - 0 °C / Inert atmosphere

4.2: 16.08 h / 20 °C / Inert atmosphere

5.1: AD-mix-β; water / tert-butyl alcohol / 3 h / 20 °C / Inert atmosphere

6.1: dmap; triethylamine / dichloromethane / 18 h / 20 °C / Inert atmosphere

7.1: sodium hydride / tetrahydrofuran / 0.67 h / 0 - 20 °C / Inert atmosphere; Cooling with ice

7.2: 3 h / 20 °C / Inert atmosphere

8.1: triethylsilane; trifluoroacetic acid / dichloromethane / 0.17 h / 20 °C / Inert atmosphere

9.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.27 h / -78 °C / Inert atmosphere

9.2: 3.02 h / Inert atmosphere; Cooling with ice

10.1: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / water; tert-butyl alcohol / 2 h / 20 °C / Inert atmosphere

10.2: 3 h / Inert atmosphere; Cooling with ice

With hydrogenchloride; triethylsilane; dmap; sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; oxalyl dichloride; AD-mix-β; potassium tert-butylate; water; sodium hydride; potassium carbonate; dimethyl sulfoxide; triethylamine; trifluoroacetic acid; magnesium chloride; In tetrahydrofuran; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; tert-butyl alcohol; 2.1: Casiraghi/Hoflokken ortho-formylation / 5.1: Sharpless dihydroxylation / 9.1: Swern oxidation / 9.2: Swern oxidation / 10.1: Lindgren-Kraus oxidation;
DOI:10.1016/j.tet.2011.04.094