C₂₆H₂₁N₂⁽¹⁺⁾*Br^(1-)

Base Information

• Chemical Name: C₂₆H₂₁N₂⁽¹⁺⁾*Br^(1-)
• CAS No.: 1613165-14-2
• Molecular Formula: Br*C₂₆H₂₁N₂
• Molecular Weight: 441.37

Synonyms:C₂₆H₂₁N₂⁽¹⁺⁾*Br^(1-)

Chemical Property of C₂₆H₂₁N₂⁽¹⁺⁾*Br^(1-)

Chemical Property:

Purity/Quality:

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Technology Process of C₂₆H₂₁N₂⁽¹⁺⁾*Br^(1-)

There total 5 articles about C₂₆H₂₁N₂⁽¹⁺⁾*Br^(1-) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

6-bromo-1-phenylpyrrolo[1,2-a]pyrazine (1613164-79-6) → C26H21N2(1+)*Br(1-) (1613165-14-2)

Guidance literature:

Multi-step reaction with 2 steps

1: palladium diacetate; potassium carbonate / ethanol; N,N-dimethyl-formamide / 0.5 h / 70 °C

2: acetone / 12 h / Reflux

With palladium diacetate; potassium carbonate; In ethanol; N,N-dimethyl-formamide; acetone;

DOI:10.1021/ol5013313

Reference yield:

1-chloropyrrolo[1,2-a]pyrazine (136927-64-5) → C26H21N2(1+)*Br(1-) (1613165-14-2)

Guidance literature:

Multi-step reaction with 4 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / benzene; ethanol; water / 80 °C / Inert atmosphere

2: 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione / tetrahydrofuran / 0.17 h / 20 °C / Inert atmosphere

3: palladium diacetate; potassium carbonate / ethanol; N,N-dimethyl-formamide / 0.5 h / 70 °C

4: acetone / 12 h / Reflux

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione; palladium diacetate; sodium carbonate; potassium carbonate; In tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide; acetone; benzene; 1: |Suzuki Coupling;

DOI:10.1021/ol5013313

Reference yield:

phenylboronic acid (98-80-6) → C26H21N2(1+)*Br(1-) (1613165-14-2)

Guidance literature:

Multi-step reaction with 4 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / benzene; ethanol; water / 80 °C / Inert atmosphere

2: 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione / tetrahydrofuran / 0.17 h / 20 °C / Inert atmosphere

3: palladium diacetate; potassium carbonate / ethanol; N,N-dimethyl-formamide / 0.5 h / 70 °C

4: acetone / 12 h / Reflux

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione; palladium diacetate; sodium carbonate; potassium carbonate; In tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide; acetone; benzene; 1: |Suzuki Coupling;

DOI:10.1021/ol5013313

upstream raw materials:

6-bromo-1-phenylpyrrolo[1,2-a]pyrazine

1,6-diphenylpyrrolo[1,2-a]pyrazine

benzyl bromide

1-Phenylpyrrolo<1,2-a>pyrazine

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