(3R,7R)-3,7,11-trimethyldodecanoic acid

Base Information

Chemical Name:(3R,7R)-3,7,11-trimethyldodecanoic acid
CAS No.:13955-73-2
Molecular Formula:C₁₅H₃₀O₂
Molecular Weight:242.402
Hs Code.:

Synonyms:(3R,7R)-3,7,11-trimethyldodecanoic acid

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Chemical Property of (3R,7R)-3,7,11-trimethyldodecanoic acid

Chemical Property:

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Technology Process of (3R,7R)-3,7,11-trimethyldodecanoic acid

There total 14 articles about (3R,7R)-3,7,11-trimethyldodecanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 6750-34-1
3,7,11-trimethyldodecyl alcohol

: 1190-55-2,13852-96-5,13955-73-2,42763-75-7,42763-79-1,57030-81-6
3R(+),7RS-3,7,11-trimethyldodecanoic acid

Guidance literature:: With Jones reagent; In isopropyl alcohol; acetone; at 0 ℃; for 4h; Inert atmosphere;
DOI:10.1055/s-0031-1289689

Reference yield:

: 1117-61-9
(3R)-citronellol

: 1190-55-2,13852-96-5,13955-73-2,42763-75-7,42763-79-1,57030-81-6
(3Ξ,7R)-3,7,11-trimethyl-dodecanoic acid

Guidance literature:: Multi-step reaction with 5 steps

1: H₂ / Pd-SrCO₃ / ethyl acetate

2: aq. HBr, H₂SO₄ / Heating

3: methanol / 168 h / Heating

4: KOH / aq. ethanol / 168 h / Heating

5: (i) NaOMe, (electrolysis), (ii) NaOH

With potassium hydroxide; sulfuric acid; hydrogen bromide; hydrogen; Pd/SrCO₃; In methanol; ethanol; ethyl acetate;
DOI:10.1039/j39660002144

Reference yield:

: 59965-20-7
(R)-1-bromo-3,7-dimethyloctane

: 1190-55-2,13852-96-5,13955-73-2,42763-75-7,42763-79-1,57030-81-6
(3Ξ,7R)-3,7,11-trimethyl-dodecanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: methanol / 168 h / Heating

2: KOH / aq. ethanol / 168 h / Heating

3: (i) NaOMe, (electrolysis), (ii) NaOH

With potassium hydroxide; In methanol; ethanol;
DOI:10.1039/j39660002144