Technology Process of C38H56O4S2
There total 3 articles about C38H56O4S2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
In
tetrahydrofuran; diethyl ether;
at -78 ℃;
for 0.5h;
Inert atmosphere;
DOI:10.1021/jm300566h
- Guidance literature:
-
Multi-step reaction with 3 steps
1: camphor-10-sulfonic acid / dichloromethane / 0.5 h / 20 °C
2: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 0.25 h / 20 °C / Molecular sieve
3: tetrahydrofuran; diethyl ether / 0.5 h / -78 °C / Inert atmosphere
With
tetrapropylammonium perruthennate; camphor-10-sulfonic acid; 4-methylmorpholine N-oxide;
In
tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1021/jm300566h
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: n-butyllithium / tetrahydrofuran; hexane / 0.75 h / 20 °C / Inert atmosphere
1.2: 2 h / 4 °C / Inert atmosphere
2.1: pyridinium p-toluenesulfonate / methanol / 17 h / 20 °C
3.1: camphor-10-sulfonic acid / dichloromethane / 0.5 h / 20 °C
4.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 0.25 h / 20 °C / Molecular sieve
5.1: tetrahydrofuran; diethyl ether / 0.5 h / -78 °C / Inert atmosphere
With
n-butyllithium; tetrapropylammonium perruthennate; camphor-10-sulfonic acid; pyridinium p-toluenesulfonate; 4-methylmorpholine N-oxide;
In
tetrahydrofuran; methanol; diethyl ether; hexane; dichloromethane;
DOI:10.1021/jm300566h
