Technology Process of C41H59BrO13
There total 9 articles about C41H59BrO13 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C65H117BrO14Si4;
With
pyridine hydrogenfluoride;
In
tetrahydrofuran;
at 0 - 20 ℃;
for 5h;
Inert atmosphere;
With
water; sodium hydrogencarbonate;
In
tetrahydrofuran; ethyl acetate;
DOI:10.1016/j.tet.2011.09.058
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: lithium triethylborohydride / tetrahydrofuran / 0 - 20 °C
2.1: 2,6-dimethylpyridine / dichloromethane / 22 h / 0 - 20 °C / Inert atmosphere
2.2: 2 h
3.1: 2,4,6-trichlorobenzoyl chloride; triethylamine / toluene / 6 h / 20 °C / Inert atmosphere
3.2: 1.5 h / 20 °C / Inert atmosphere
4.1: pyridine hydrogenfluoride / tetrahydrofuran / 5 h / 0 - 20 °C / Inert atmosphere
With
2,6-dimethylpyridine; 2,4,6-trichlorobenzoyl chloride; lithium triethylborohydride; pyridine hydrogenfluoride; triethylamine;
In
tetrahydrofuran; dichloromethane; toluene;
DOI:10.1016/j.tet.2011.09.058
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: 2,4,6-trichlorobenzoyl chloride; triethylamine / toluene / 6 h / 20 °C / Inert atmosphere
1.2: 1.5 h / 20 °C / Inert atmosphere
2.1: pyridine hydrogenfluoride / tetrahydrofuran / 5 h / 0 - 20 °C / Inert atmosphere
With
2,4,6-trichlorobenzoyl chloride; pyridine hydrogenfluoride; triethylamine;
In
tetrahydrofuran; toluene;
DOI:10.1016/j.tet.2011.09.058
