5-(13-[(2S,3S)-3-((R)-1-methylheptadecyl)oxiranyl]tridecane-1-sulfonyl)-1-phenyl-1H-tetrazole

Base Information

• Chemical Name: 5-(13-[(2S,3S)-3-((R)-1-methylheptadecyl)oxiranyl]tridecane-1-sulfonyl)-1-phenyl-1H-tetrazole
• CAS No.: 1221891-97-9
• Molecular Formula: C₄₀H₇₀N₄O₃S
• Molecular Weight: 687.087

Synonyms:5-(13-[(2S,3S)-3-((R)-1-methylheptadecyl)oxiranyl]tridecane-1-sulfonyl)-1-phenyl-1H-tetrazole

Chemical Property of 5-(13-[(2S,3S)-3-((R)-1-methylheptadecyl)oxiranyl]tridecane-1-sulfonyl)-1-phenyl-1H-tetrazole

Chemical Property:

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Technology Process of 5-(13-[(2S,3S)-3-((R)-1-methylheptadecyl)oxiranyl]tridecane-1-sulfonyl)-1-phenyl-1H-tetrazole

There total 3 articles about 5-(13-[(2S,3S)-3-((R)-1-methylheptadecyl)oxiranyl]tridecane-1-sulfonyl)-1-phenyl-1H-tetrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

5-(13-[(2S,3S)-3-((R)-1-methyl-heptadecyl)oxiranyl]tridecylsulfanyl)-1-phenyl-1H-tetrazole (1221892-10-9) → 5-(13-[(2S,3S)-3-((R)-1-methylheptadecyl)oxiranyl]tridecane-1-sulfonyl)-1-phenyl-1H-tetrazole (1221891-97-9)

Guidance literature:

With 1H-imidazole; ammonium heptamolybdate monohydrate; dihydrogen peroxide; In tetrahydrofuran;

DOI:10.1016/j.tetlet.2010.01.078

Reference yield:

(E/Z)-(2S,3S)-2-(13-bromotridec-1-enyl)-3-((R)-1-methylheptadecyl)oxirane → 5-(13-[(2S,3S)-3-((R)-1-methylheptadecyl)oxiranyl]tridecane-1-sulfonyl)-1-phenyl-1H-tetrazole (1221891-97-9)

Guidance literature:

Multi-step reaction with 3 steps

1: potassium diazodicarboxylate; acetic acid / methanol; tetrahydrofuran / 0 - 20 °C / Inert atmosphere

2: potassium carbonate / acetone / 2.5 h / Reflux

3: dihydrogen peroxide; ammonium molybdate (VI) tetrahydrate / tetrahydrofuran; water / 20 h / 12 - 20 °C

With ammonium molybdate (VI) tetrahydrate; dihydrogen peroxide; potassium diazodicarboxylate; potassium carbonate; acetic acid; In tetrahydrofuran; methanol; water; acetone;

DOI:10.1016/j.tet.2014.06.089

Reference yield:

(2S,3S)-2-(13-bromotridecyl)-3-((R)-1-methylheptadecyl)oxirane (1221891-96-8) + 1-Phenyl-1H-tetrazole-5-thiol (86-93-1) → 5-(13-[(2S,3S)-3-((R)-1-methylheptadecyl)oxiranyl]tridecane-1-sulfonyl)-1-phenyl-1H-tetrazole (1221891-97-9)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / acetone / 2.5 h / Reflux

2: dihydrogen peroxide; ammonium molybdate (VI) tetrahydrate / tetrahydrofuran; water / 20 h / 12 - 20 °C

With ammonium molybdate (VI) tetrahydrate; dihydrogen peroxide; potassium carbonate; In tetrahydrofuran; water; acetone;

DOI:10.1016/j.tet.2014.06.089

upstream raw materials:

5-(13-[(2S,3S)-3-((R)-1-methyl-heptadecyl)oxiranyl]tridecylsulfanyl)-1-phenyl-1H-tetrazole

(2S,3S)-2-(13-bromotridecyl)-3-((R)-1-methylheptadecyl)oxirane

1-Phenyl-1H-tetrazole-5-thiol

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