4-Chloro-benzenesulfonic acid; compound with 4-chloro-phenylamine

Base Information

• Chemical Name: 4-Chloro-benzenesulfonic acid; compound with 4-chloro-phenylamine
• CAS No.: 53039-76-2
• Molecular Formula: C₆H₅ClO₃S*C₆H₆ClN
• Molecular Weight: 320.196
• Mol file: 53039-76-2.mol

Synonyms:4-Chloro-benzenesulfonic acid; compound with 4-chloro-phenylamine

Chemical Property of 4-Chloro-benzenesulfonic acid; compound with 4-chloro-phenylamine

Chemical Property:

Purity/Quality:

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Technology Process of 4-Chloro-benzenesulfonic acid; compound with 4-chloro-phenylamine

There total 11 articles about 4-Chloro-benzenesulfonic acid; compound with 4-chloro-phenylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl p-chlorobenzenesulphonate (15481-45-5) + 4-chloro-aniline (106-47-8) → N-methyl(p-chloroaniline) (932-96-7) + 4-Chloro-benzenesulfonic acid; compound with 4-chloro-phenylamine (53039-76-2)

Guidance literature:

In methanol; at 65 ℃;

Reference yield:

4-chloro-aniline (106-47-8) + 4-Chloro-benzenesulfonic acid cyclobutylmethyl ester (191664-01-4) → 4-Chloro-benzenesulfonic acid; compound with 4-chloro-phenylamine (53039-76-2) + (4-Chloro-phenyl)-cyclobutylmethyl-amine

Guidance literature:

In methanol; at 65 ℃; Rate constant;

DOI:10.1002/(SICI)1099-1395(199702)10:2<91::AID-POC862>3.0.CO;2-M

Reference yield:

ethyl chlorobenzene-p-sulphonate (20443-71-4) + 4-chloro-aniline (106-47-8) → N-ethyl-4-chloro-aniline (13519-75-0) + 4-Chloro-benzenesulfonic acid; compound with 4-chloro-phenylamine (53039-76-2)

Guidance literature:

In methanol; at 65 ℃;

upstream raw materials:

ethyl chlorobenzene-p-sulphonate

4-chloro-aniline

methyl p-chlorobenzenesulphonate

4-Chloro-benzenesulfonic acid 1-methyl-1-phenyl-ethyl ester