isonicotinic acid-2-acetyl-3,5-dimethoxyphenyl ester

Base Information

Chemical Name:isonicotinic acid-2-acetyl-3,5-dimethoxyphenyl ester
CAS No.:92964-08-4
Molecular Formula:C₁₆H₁₅NO₅
Molecular Weight:301.299
Hs Code.:

Synonyms:isonicotinic acid-2-acetyl-3,5-dimethoxyphenyl ester

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Chemical Property of isonicotinic acid-2-acetyl-3,5-dimethoxyphenyl ester

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Technology Process of isonicotinic acid-2-acetyl-3,5-dimethoxyphenyl ester

There total 1 articles about isonicotinic acid-2-acetyl-3,5-dimethoxyphenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 55-22-1
pyridine-4-carboxylic acid

: 90-24-4
2-hydroxy-4,6-dimethoxyacetophenone

: 92964-08-4
isonicotinic acid-2-acetyl-3,5-dimethoxyphenyl ester

Guidance literature:: With pyridine; trichlorophosphate; at 0 - 20 ℃; for 16h;

Reference yield: 88.0%

: 92964-08-4
isonicotinic acid-2-acetyl-3,5-dimethoxyphenyl ester

: 6344-88-3
1-(2-hydroxy-4,6-dimethoxy-phenyl)-3-pyridin-4-yl-propane-1,3-dione

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; at 20 ℃; for 24h;

Reference yield:

: 92964-08-4
isonicotinic acid-2-acetyl-3,5-dimethoxyphenyl ester

: 2-((benzyl(methyl)amino)methyl)-3,5-dimethoxy-6-(5-(pyridin-4-yl)-1H-pyrazol-3-yl)phenol

Guidance literature:: Multi-step reaction with 4 steps

1: potassium hydroxide / N,N-dimethyl-formamide / 2 h

2: sulfuric acid / acetic acid / 2 h / 100 °C

3: hydrazine hydrate / methanol / 10 h / Reflux

4: 1,4-dioxane / 60 °C

With sulfuric acid; hydrazine hydrate; potassium hydroxide; In 1,4-dioxane; methanol; acetic acid; N,N-dimethyl-formamide; 1: |Baker-Venkataraman Rearrangement / 4: |Mannich Aminomethylation;
DOI:10.1111/cbdd.12489