benzyl 4-O-benzyl-2,3-O-methylene-4-C-vinyl-6-deoxy-α-D-galactopyranoside

Base Information

Chemical Name:benzyl 4-O-benzyl-2,3-O-methylene-4-C-vinyl-6-deoxy-α-D-galactopyranoside
CAS No.:77977-27-6
Molecular Formula:C₂₃H₂₆O₅
Molecular Weight:382.456
Hs Code.:

Synonyms:benzyl 4-O-benzyl-2,3-O-methylene-4-C-vinyl-6-deoxy-α-D-galactopyranoside

Suppliers and Price of benzyl 4-O-benzyl-2,3-O-methylene-4-C-vinyl-6-deoxy-α-D-galactopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of benzyl 4-O-benzyl-2,3-O-methylene-4-C-vinyl-6-deoxy-α-D-galactopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of benzyl 4-O-benzyl-2,3-O-methylene-4-C-vinyl-6-deoxy-α-D-galactopyranoside

There total 1 articles about benzyl 4-O-benzyl-2,3-O-methylene-4-C-vinyl-6-deoxy-α-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 100-44-7
benzyl chloride

: 76820-24-1
benzyl 6-deoxy-2,3-O-methylene-4-C-vinyl-α-D-galactopyranoside

: 77977-27-6
benzyl 4-O-benzyl-2,3-O-methylene-4-C-vinyl-6-deoxy-α-D-galactopyranoside

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; for 2h; Ambient temperature;
DOI:10.1016/S0008-6215(00)84690-X

Reference yield: 28.9%

: 77977-27-6
benzyl 4-O-benzyl-2,3-O-methylene-4-C-vinyl-6-deoxy-α-D-galactopyranoside

: 80018-86-6,80018-87-7
(3aR,4S,6R,7R,7aR)-4,7-Bis-benzyloxy-6-methyl-7-(S)-oxiranyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran

: 80018-86-6,80018-87-7
(3aR,4S,6R,7R,7aR)-4,7-Bis-benzyloxy-6-methyl-7-(R)-oxiranyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In 1,2-dichloro-ethane; at 80 - 90 ℃; for 48h;
DOI:10.1016/S0008-6215(00)84690-X

Reference yield:

: 77977-27-6
benzyl 4-O-benzyl-2,3-O-methylene-4-C-vinyl-6-deoxy-α-D-galactopyranoside

: 77977-29-8
benzyl 4-O-benzyl-6-deoxy-4-C-<(S)-1-hydroxyethyl>-2,3-O-methylene-α-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 57.6 percent / m-chloroperbenzoic acid / 1,2-dichloro-ethane / 48 h / 80 - 90 °C

2: 89 percent / lithium aluminum hidride, oxolane / 2 h / Ambient temperature

With tetrahydrofuran; lithium aluminium tetrahydride; 3-chloro-benzenecarboperoxoic acid; In 1,2-dichloro-ethane;
DOI:10.1016/S0008-6215(00)84690-X