Technology Process of C35H40F4N4O6S
There total 14 articles about C35H40F4N4O6S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tetrakis(triphenylphosphine) palladium(0); potassium carbonate;
In
1,2-dimethoxyethane; water;
at 90 ℃;
for 3h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: lithium hydroxide; water / tetrahydrofuran / 2 h / 0 - 20 °C
2: triethylamine / dichloromethane / 3 h / 0 - 20 °C
3: ammonium acetate / toluene / 5 h / 110 °C
4: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium acetate / N,N-dimethyl-formamide / 2 h / 90 °C / Inert atmosphere
5: hydrogenchloride / ethyl acetate / 8 h / 20 °C
6: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 3 h / 0 - 20 °C
7: potassium carbonate; tetrakis(triphenylphosphine) palladium(0) / 1,2-dimethoxyethane; water / 3 h / 90 °C / Inert atmosphere
With
hydrogenchloride; tetrakis(triphenylphosphine) palladium(0); dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; ammonium acetate; water; potassium acetate; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; lithium hydroxide;
In
tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; toluene;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: potassium tert-butylate / toluene / 2.5 h / 0 - 110 °C / Inert atmosphere
2.1: trifluoroacetic acid; triethylsilane / 7 h / 0 - 40 °C / Inert atmosphere
3.1: boron tribromide / dichloromethane / 1.16 h / -78 - 20 °C
4.1: pyridine / dichloromethane / 0.02 h / 0 °C
4.2: 1 h / 0 - 20 °C
5.1: potassium carbonate; tetrakis(triphenylphosphine) palladium(0) / 1,2-dimethoxyethane; water / 3 h / 90 °C / Inert atmosphere
With
pyridine; triethylsilane; tetrakis(triphenylphosphine) palladium(0); potassium tert-butylate; boron tribromide; potassium carbonate; trifluoroacetic acid;
In
1,2-dimethoxyethane; dichloromethane; water; toluene;