2,5-bis(trideuteriomethyl)-1,4-hydroquinone-O,O'-bis(N,N'-diethylcarbamate)

Base Information

Chemical Name:2,5-bis(trideuteriomethyl)-1,4-hydroquinone-O,O'-bis(N,N'-diethylcarbamate)
CAS No.:203579-46-8
Molecular Formula:C₁₈H₂₈N₂O₄
Molecular Weight:342.384
Hs Code.:

Synonyms:2,5-bis(trideuteriomethyl)-1,4-hydroquinone-O,O'-bis(N,N'-diethylcarbamate)

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Chemical Property of 2,5-bis(trideuteriomethyl)-1,4-hydroquinone-O,O'-bis(N,N'-diethylcarbamate)

Chemical Property:

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Technology Process of 2,5-bis(trideuteriomethyl)-1,4-hydroquinone-O,O'-bis(N,N'-diethylcarbamate)

There total 1 articles about 2,5-bis(trideuteriomethyl)-1,4-hydroquinone-O,O'-bis(N,N'-diethylcarbamate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 865-50-9
iodomethane-d3

: 97567-55-0
O-(4-N,N-diethylcarbamoyloxy)phenyl N,N-diethylcarbamate

: 203579-46-8
2,5-bis(trideuteriomethyl)-1,4-hydroquinone-O,O'-bis(N,N'-diethylcarbamate)

Guidance literature:: With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In tetrahydrofuran; hexane; cyclohexane; at -78 ℃; to RT;

Reference yield:

: 203579-46-8
2,5-bis(trideuteriomethyl)-1,4-hydroquinone-O,O'-bis(N,N'-diethylcarbamate)

: 203579-70-8
2,5-bis(trideuteriomethyl)-1,4-benzoquinone

Guidance literature:: Multi-step reaction with 2 steps

1: NaOH / H₂O; methanol / 96 h / Heating

2: CrO₃, H₂SO₄ / acetone; H₂O / 0.5 h / 0 °C

With chromium(VI) oxide; sodium hydroxide; sulfuric acid; In methanol; water; acetone;

Reference yield:

: 203579-46-8
2,5-bis(trideuteriomethyl)-1,4-hydroquinone-O,O'-bis(N,N'-diethylcarbamate)

: N,N'-dicyano-2,5-bis(trideuteriomethyl)-1,4-benzoquinone diimine

Guidance literature:: Multi-step reaction with 3 steps

1: NaOH / H₂O; methanol / 96 h / Heating

2: CrO₃, H₂SO₄ / acetone; H₂O / 0.5 h / 0 °C

3: 84 percent / TiCl₄ / CH₂Cl₂ / 16 h / 20 °C

With chromium(VI) oxide; sodium hydroxide; sulfuric acid; titanium tetrachloride; In methanol; dichloromethane; water; acetone;